1-benzyl-6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(1H)-one

Base Information

Chemical Name:1-benzyl-6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(1H)-one
CAS No.:135119-44-7
Molecular Formula:C₂₃H₃₀N₄OS
Molecular Weight:410.583
Hs Code.:

1-benzyl-6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<d><1,2,4>triazolo<1,5-a>pyrimidin-5(1H)-one

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Chemical Property of 1-benzyl-6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(1H)-one

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Technology Process of 1-benzyl-6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(1H)-one

There total 3 articles about 1-benzyl-6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 100-44-7
benzyl chloride

: 6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(16H)-one tetrabutylammonium salt

: 135119-46-9
16-benzyl-6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(16H)-one

: 135119-45-8
3-benzyl-6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(3H)-one

: 135119-44-7
1-benzyl-6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(1H)-one

Guidance literature:: In acetonitrile; for 1.5h; Heating;

Reference yield:

: 135119-42-5
6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(16H)-one

: 135119-44-7
1-benzyl-6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / aq. NaOH / CHCl₃

2: 24 percent / acetonitrile / 1 h / Heating

With sodium hydroxide; In chloroform; acetonitrile;
DOI:10.1002/jhet.5570380136

Reference yield:

: 4017-60-1,75232-70-1
ethyl 2-oxocyclododecane-1-carboxylate

: 135119-44-7
1-benzyl-6,7,8,9,10,11,12,13,14,15-decahydro-2-methylthiocyclododeca<1,2,4>triazolo<1,5-a>pyrimidin-5(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / acetic acid / 5 h / Heating; or 180 - 190 deg C, 10 min

2: NaOH / H₂O / below 10 deg C

3: 30 percent / acetonitrile / 1.5 h / Heating

With sodium hydroxide; acetic acid; In water; acetonitrile;