8-Benzyliden-2,6,7,8-tetrahydrocyclopentano-1,2-diazepin-2-carbonsaeure-ethylester

Base Information

• Chemical Name: 8-Benzyliden-2,6,7,8-tetrahydrocyclopentano-1,2-diazepin-2-carbonsaeure-ethylester
• CAS No.: 111113-99-6
• Molecular Formula: C₁₈H₁₈N₂O₂
• Molecular Weight: 294.353
• Mol file: 111113-99-6.mol

Synonyms:

Chemical Property of 8-Benzyliden-2,6,7,8-tetrahydrocyclopentano-1,2-diazepin-2-carbonsaeure-ethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 8-Benzyliden-2,6,7,8-tetrahydrocyclopentano-1,2-diazepin-2-carbonsaeure-ethylester

There total 3 articles about 8-Benzyliden-2,6,7,8-tetrahydrocyclopentano-1,2-diazepin-2-carbonsaeure-ethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

7-Benzyliden-5,6-dihydro-7H-cyclopentapyridinium-1-(ethoxycarbonylaminid) (111113-90-7) → 8-Benzyliden-2,6,7,8-tetrahydrocyclopentano-1,2-diazepin-2-carbonsaeure-ethylester (111113-99-6)

Guidance literature:

In benzene; at 10 - 15 ℃; Irradiation;

Reference yield:

7-Benzyliden-6,7-dihydro-5H-1-pyrindin (74701-35-2) → 8-Benzyliden-2,6,7,8-tetrahydrocyclopentano-1,2-diazepin-2-carbonsaeure-ethylester (111113-99-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / CH₂Cl₂ / 1 h / Ambient temperature

2: 48 percent / 10percent KOH / ethanol / 12 h / Ambient temperature

3: 47 percent / benzene / 10 - 15 °C / Irradiation

With potassium hydroxide; In ethanol; dichloromethane; benzene;

Reference yield:

1-Amino-7-benzyliden-5,6-dihydro-7H-cyclopentapyridinium-mesitylensulfonat (111113-94-1) → 8-Benzyliden-2,6,7,8-tetrahydrocyclopentano-1,2-diazepin-2-carbonsaeure-ethylester (111113-99-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 48 percent / 10percent KOH / ethanol / 12 h / Ambient temperature

2: 47 percent / benzene / 10 - 15 °C / Irradiation

With potassium hydroxide; In ethanol; benzene;

upstream raw materials:

7-Benzyliden-5,6-dihydro-7H-cyclopentapyridinium-1-(ethoxycarbonylaminid)

7-Benzyliden-6,7-dihydro-5H-1-pyrindin

1-Amino-7-benzyliden-5,6-dihydro-7H-cyclopentapyridinium-mesitylensulfonat