diethyl 1-(o-nitrobenzoyl)pyrrolo<2,3-c>pyridine-2,5-dicarboxylate

Base Information

Chemical Name:diethyl 1-(o-nitrobenzoyl)pyrrolo<2,3-c>pyridine-2,5-dicarboxylate
CAS No.:122631-08-7
Molecular Formula:C₂₀H₁₇N₃O₇
Molecular Weight:411.371
Hs Code.:

Synonyms:

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Chemical Property of diethyl 1-(o-nitrobenzoyl)pyrrolo<2,3-c>pyridine-2,5-dicarboxylate

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Technology Process of diethyl 1-(o-nitrobenzoyl)pyrrolo<2,3-c>pyridine-2,5-dicarboxylate

There total 8 articles about diethyl 1-(o-nitrobenzoyl)pyrrolo<2,3-c>pyridine-2,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5832-38-2
4-methyl-5-nitropyridine-2-carboxaldehyde

: 122631-08-7
diethyl 1-(o-nitrobenzoyl)pyrrolo<2,3-c>pyridine-2,5-dicarboxylate

Guidance literature:: Multi-step reaction with 7 steps

1: 89 percent / p-toluenesulfonic acid monohydrate / toluene / Heating

2: 1.) potassium, ethanol / 1.) room temperature, 15 min, 2.) toluene, room temperature, 2 h

3: 62 percent / H₂ / 10percent Pd/C / CH₂Cl₂ / 2 h / 1551.4 Torr

4: 77 percent / p-toluenesulfonic acid monohydrate / acetonitrile; H₂O / 5 h / Heating

5: 89 percent / 33percent H₂O₂, formic acid / H₂O / 4 °C

6: 95 percent / HCl / 6 h / Heating

7: 1.) NaH, KI / 1.) THF, room temperature, 2 h, 2.) room temperature, 30 min

With hydrogenchloride; formic acid; ethanol; hydrogen; dihydrogen peroxide; potassium; sodium hydride; toluene-4-sulfonic acid; potassium iodide; palladium on activated charcoal; In dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 108-47-4
2,4-lutidine

: 122631-08-7
diethyl 1-(o-nitrobenzoyl)pyrrolo<2,3-c>pyridine-2,5-dicarboxylate

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) KNO₃, H₂SO₄, 2.) (C₆H₅SeO)2O / 1.) 0 deg C, 1 h, room temperature, 2 h; 100 deg C, 5 h; 130 deg C, 4h, 2.) dioxane, reflux

2: 89 percent / p-toluenesulfonic acid monohydrate / toluene / Heating

3: 1.) potassium, ethanol / 1.) room temperature, 15 min, 2.) toluene, room temperature, 2 h

4: 62 percent / H₂ / 10percent Pd/C / CH₂Cl₂ / 2 h / 1551.4 Torr

5: 77 percent / p-toluenesulfonic acid monohydrate / acetonitrile; H₂O / 5 h / Heating

6: 89 percent / 33percent H₂O₂, formic acid / H₂O / 4 °C

7: 95 percent / HCl / 6 h / Heating

8: 1.) NaH, KI / 1.) THF, room temperature, 2 h, 2.) room temperature, 30 min

With hydrogenchloride; formic acid; ethanol; sulfuric acid; benzeneseleninic anhydride; hydrogen; dihydrogen peroxide; potassium; sodium hydride; toluene-4-sulfonic acid; potassium nitrate; potassium iodide; palladium on activated charcoal; In dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 119694-70-1
2-(1,3-dioxolan-2-yl)-4-methyl-5-nitropyridine

: 122631-08-7
diethyl 1-(o-nitrobenzoyl)pyrrolo<2,3-c>pyridine-2,5-dicarboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) potassium, ethanol / 1.) room temperature, 15 min, 2.) toluene, room temperature, 2 h

2: 62 percent / H₂ / 10percent Pd/C / CH₂Cl₂ / 2 h / 1551.4 Torr

3: 77 percent / p-toluenesulfonic acid monohydrate / acetonitrile; H₂O / 5 h / Heating

4: 89 percent / 33percent H₂O₂, formic acid / H₂O / 4 °C

5: 95 percent / HCl / 6 h / Heating

6: 1.) NaH, KI / 1.) THF, room temperature, 2 h, 2.) room temperature, 30 min

With hydrogenchloride; formic acid; ethanol; hydrogen; dihydrogen peroxide; potassium; sodium hydride; toluene-4-sulfonic acid; potassium iodide; palladium on activated charcoal; In dichloromethane; water; acetonitrile;