1-(Phenylselanyl)butan-2-one

Base Information

Chemical Name:1-(Phenylselanyl)butan-2-one
CAS No.:109297-37-2
Molecular Formula:C10H12OSe
Molecular Weight:227.165
Hs Code.:
DSSTox Substance ID:DTXSID50546125
Nikkaji Number:J812.054D
Wikidata:Q82423846
Mol file:109297-37-2.mol

Synonyms:109297-37-2;1-(Phenylselanyl)butan-2-one;DTXSID50546125

Suppliers and Price of 1-(Phenylselanyl)butan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1-(Phenylselanyl)butan-2-one

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:228.00534
Heavy Atom Count:12
Complexity:139

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(=O)C[Se]C1=CC=CC=C1

Technology Process of 1-(Phenylselanyl)butan-2-one

There total 4 articles about 1-(Phenylselanyl)butan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41924-21-4
phenyl tributylstannyl selenide

: 816-40-0
1-Bromo-2-butanone

: 109297-37-2
1-phenylselanylbutan-2-one

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 80 ℃; for 6h;
DOI:10.1021/jo026894i

Reference yield:

: 645-96-5
Benzeneselenol

: 109297-37-2
1-phenylselanylbutan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / SO₂Cl₂ / petroleum ether; CHCl₃ / 0.5 h

2: 2.) thiourea, H₂O / 1.) CH₃CN, -30 deg C, 480 min, 2.) acetone, CH₂Cl₂

With sulfuryl dichloride; water; thiourea; In chloroform; Petroleum ether;
DOI:10.1055/s-1997-1509

Reference yield:

: 1666-13-3
diphenyl diselenide

: 14091-67-9
1-(trimethylsilyl)-2-butanone

: 109297-37-2
1-phenylselanylbutan-2-one

Guidance literature:: With bromine; zinc dibromide; Yield given. Multistep reaction; 2.) CH₂Cl₂, -78 deg C, 15 min;
DOI:10.1016/0022-328X(86)80349-7