Ru₃H₂S((CH)2(P(C₆H₅)2)2)(CO)7

Base Information

• Chemical Name: Ru₃H₂S((CH)2(P(C₆H₅)2)2)(CO)7
• CAS No.: 105159-52-2
• Molecular Formula: C₃₃H₂₄O₇P₂Ru₃S
• Molecular Weight: 929.773

Synonyms:

Chemical Property of Ru₃H₂S((CH)2(P(C₆H₅)2)2)(CO)7

Chemical Property:

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Technology Process of Ru₃H₂S((CH)2(P(C₆H₅)2)2)(CO)7

There total 1 articles about Ru₃H₂S((CH)2(P(C₆H₅)2)2)(CO)7 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(μ-H)2Ru3(μ3-S)(CO)9 + 1,2-bis(diphenylphosphino)ethylene (17427-91-7) → Ru3H2S((CH)2(P(C6H5)2)2)(CO)7 (105159-52-2)

Guidance literature:

With catalyst: (C₆H₅)6P₂N(OOCCH₃); In tetrahydrofuran; catalyst was added to the soln. of Ru complex and ligand in THF, mixt. was heated to reflux for 30 min; chromy., recrystd. from CH2Cl2/methanol, elem. anal.;

upstream raw materials:

1,2-bis(diphenylphosphino)ethylene

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