C₁₅H₉FIN₃O₂

Base Information

• Chemical Name: C₁₅H₉FIN₃O₂
• CAS No.: 1332882-50-4
• Molecular Formula: C₁₅H₉FIN₃O₂
• Molecular Weight: 409.158
• Mol file: 1332882-50-4.mol

Synonyms:

Chemical Property of C₁₅H₉FIN₃O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₉FIN₃O₂

There total 6 articles about C₁₅H₉FIN₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 3-fluorobenzoate (451-02-5) → C15H9FIN3O2 (1332882-50-4)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / 6 h / Reflux

2: acetic acid / ethanol; water / 6 h / Reflux

With hydrazine hydrate; acetic acid; In ethanol; water;

DOI:10.1021/jf2021607

Reference yield:

2-iodophenylamine (615-43-0) → C15H9FIN3O2 (1332882-50-4)

Guidance literature:

Multi-step reaction with 4 steps

1: hydrogenchloride; sodium sulfate / water / 0.9 h / 40 °C

2: hydroxylamine hydrochloride / water / 4 h / 40 - 75 °C

3: sulfuric acid / water / 75 - 80 °C

4: acetic acid / ethanol; water / 6 h / Reflux

With hydrogenchloride; sulfuric acid; hydroxylamine hydrochloride; acetic acid; sodium sulfate; In ethanol; water;

DOI:10.1021/jf2021607

Reference yield:

2'-hydroxyimino-2-iodoacetanilide (117500-16-0) → C15H9FIN3O2 (1332882-50-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / water / 75 - 80 °C

2: acetic acid / ethanol; water / 6 h / Reflux

With sulfuric acid; acetic acid; In ethanol; water;

DOI:10.1021/jf2021607

upstream raw materials:

C₈H₅Cl₃INO

7-iodoisatin

3-fluoro-benzoic acid hydrazide

3-fluorobenzoic acid