1-methyl-2-cyano-5-methoxy-3-benzylbenzindole

Base Information

Chemical Name:1-methyl-2-cyano-5-methoxy-3-benzylbenzindole
CAS No.:132205-87-9
Molecular Formula:C₂₂H₁₈N₂O
Molecular Weight:326.398
Hs Code.:

1-methyl-2-cyano-5-methoxy-3-benzylbenz<e>indole

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-methyl-2-cyano-5-methoxy-3-benzylbenzindole

Chemical Property:

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Technology Process of 1-methyl-2-cyano-5-methoxy-3-benzylbenzindole

There total 3 articles about 1-methyl-2-cyano-5-methoxy-3-benzylbenzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.3%

: 143-33-9,25596-52-5
sodium cyanide

: (3-Benzyl-5-methoxy-3H-benzo[e]indol-1-ylmethyl)-trimethyl-ammonium; iodide

: 132205-87-9
1-methyl-2-cyano-5-methoxy-3-benzylbenzindole

: 132205-86-8
5-methoxy-3-benzylbenzindole-1-acetonitrile

Guidance literature:: In N,N-dimethyl-formamide; for 4h; Heating;
DOI:10.1021/jo00006a052

Reference yield:

: 132205-82-4
5-methoxy-3-benzyl-3H-benzindole

: 132205-87-9
1-methyl-2-cyano-5-methoxy-3-benzylbenzindole

Guidance literature:: Multi-step reaction with 3 steps

1: 35.6 percent / glacial acetic acid / 1.) 0 deg C -> room temperature, 2.) 4 h

2: 89.7 percent / benzene

3: 27.1 percent / dimethylformamide / 4 h / Heating

With acetic acid; In N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00006a052

Reference yield:

: 132205-84-6
(3-Benzyl-5-methoxy-3H-benzo[e]indol-1-ylmethyl)-dimethyl-amine

: 132205-87-9
1-methyl-2-cyano-5-methoxy-3-benzylbenzindole

Guidance literature:: Multi-step reaction with 2 steps

1: 89.7 percent / benzene

2: 27.1 percent / dimethylformamide / 4 h / Heating

In N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00006a052