trans-N-<2-<2'-cyclopentyl>ethyl>-N-methyl-p-nitroaniline

Base Information

Chemical Name:trans-N-<2-<2'-cyclopentyl>ethyl>-N-methyl-p-nitroaniline
CAS No.:121374-61-6
Molecular Formula:C₂₂H₂₇N₃O₄
Molecular Weight:397.474
Hs Code.:

trans-N-<2-<2'-<N'-(carbobenzyloxy)amino>cyclopentyl>ethyl>-N-methyl-p-nitroaniline

Synonyms:

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Chemical Property of trans-N-<2-<2'-cyclopentyl>ethyl>-N-methyl-p-nitroaniline

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Technology Process of trans-N-<2-<2'-cyclopentyl>ethyl>-N-methyl-p-nitroaniline

There total 4 articles about trans-N-<2-<2'-cyclopentyl>ethyl>-N-methyl-p-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121374-59-2,121374-60-5
N-<2-(2'-oxocyclopentyl)ethyl>-N-methyl-p-nitroaniline oxime O-methyl ether

: 121374-61-6,121374-62-7
cis-N-<2-<2'-cyclopentyl>ethyl>-N-methyl-p-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: sodium borohydride, trifluoroacetic acid / tetrahydrofuran / 18 h / Heating

2: 1 M NaOH / diethyl ether / 18 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; trifluoroacetic acid; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00275a034

Reference yield:

: 121374-59-2,121374-60-5
N-<2-(2'-oxocyclopentyl)ethyl>-N-methyl-p-nitroaniline oxime O-methyl ether

: 121374-61-6,121374-62-7
trans-N-<2-<2'-cyclopentyl>ethyl>-N-methyl-p-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: sodium borohydride, trifluoroacetic acid / tetrahydrofuran / 18 h / Heating

2: 1 M NaOH / diethyl ether / 18 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; trifluoroacetic acid; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00275a034

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 121375-01-7
[2-(2-Amino-cyclopentyl)-ethyl]-methyl-(4-nitro-phenyl)-amine

: 121374-61-6,121374-62-7
cis-N-<2-<2'-cyclopentyl>ethyl>-N-methyl-p-nitroaniline

: 121374-61-6,121374-62-7
trans-N-<2-<2'-cyclopentyl>ethyl>-N-methyl-p-nitroaniline

Guidance literature:: With sodium hydroxide; In diethyl ether; for 18h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo00275a034