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Technology Process of 3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside

3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside

Base Information
  • Chemical Name:3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside
  • CAS No.:134662-23-0
  • Molecular Formula:C107H117NO22
  • Molecular Weight:1769.1
  • Hs Code.:
3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside

Synonyms:

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Chemical Property of 3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside
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Technology Process of 3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside

There total 1 articles about 3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-[(N-benzyloxycarbonyl)amino]propanol
34637-22-4

3-[(N-benzyloxycarbonyl)amino]propanol

ethyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-1-thio-α-L-rhamnopyranoside
134662-22-9

ethyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-1-thio-α-L-rhamnopyranoside

C<sub>96</sub>H<sub>104</sub>O<sub>20</sub>

C96H104O20

3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside
134662-23-0,134732-29-9

3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside

Guidance literature:
With silver silicate; bromine; Yield given. Multistep reaction; 1) CH2Cl2, 10 min; 2) toluene, CH2Cl2, 2 h;
DOI:10.1016/0008-6215(91)80096-6

Reference yield: 98.0%

3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside
134662-23-0,134732-29-9

3-benzyloxycarbonylaminopropyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-α,β-L-rhamnopyranoside

3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-α,β-L-rhamnopyranoside
134662-24-1,134732-30-2

3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-α,β-L-rhamnopyranoside

Guidance literature:
With sodium methylate; In methanol; dichloromethane; for 48h;
DOI:10.1016/0008-6215(91)80096-6
upstream raw materials:

3-[(N-benzyloxycarbonyl)amino]propanol

ethyl 4-O-<3-O-acetyl-6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-2,3-di-O-benzyl-1-thio-α-L-rhamnopyranoside

Downstream raw materials:

3-benzyloxycarbonylaminopropyl 2,3-di-O-benzyl-4-O-<6-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-D-galactopyranosyl>-α,β-L-rhamnopyranoside

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