C₂₄H₂₅F₃O₃

Base Information

Chemical Name:C₂₄H₂₅F₃O₃
CAS No.:1390635-59-2
Molecular Formula:C₂₄H₂₅F₃O₃
Molecular Weight:418.456
Hs Code.:

C<sub>24</sub>H<sub>25</sub>F<sub>3</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₅F₃O₃

Chemical Property:

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Technology Process of C₂₄H₂₅F₃O₃

There total 7 articles about C₂₄H₂₅F₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1390635-54-7
C₁₄H₁₈O

: 39637-99-5,20445-33-4
(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

: 1390635-59-2
C₂₄H₂₅F₃O₃

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;
DOI:10.5012/bkcs.2012.33.6.2055

Reference yield:

: 13175-44-5
oct-7-en-1-ol

: 1390635-59-2
C₂₄H₂₅F₃O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

1.2: -78 - 20 °C

2.1: triphenylphosphine / dichloromethane / 0 °C

2.2: -78 - 20 °C

3.1: tetrahydrofuran / -78 - 20 °C

4.1: Lindlar's catalyst; hydrogen / ethyl acetate; cyclohexene / 20 °C

5.1: methyllithium lithium bromide / tetrahydrofuran / 2 h / 0 - 20 °C

5.2: 0.17 h / 0 °C

6.1: Amano Lipase AK / hexane / 16 h / 20 °C / Molecular sieve; Inert atmosphere; Enzymatic reaction

7.1: water; lithium hydroxide / tetrahydrofuran / 5 h / 20 °C

8.1: pyridine / dichloromethane / 20 °C

With pyridine; oxalyl dichloride; methyllithium lithium bromide; Amano Lipase AK; Lindlar's catalyst; water; hydrogen; dimethyl sulfoxide; triphenylphosphine; lithium hydroxide; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate; cyclohexene; 1.1: Swern oxidation / 1.2: Swern oxidation / 2.1: Corey-Fuchs reaction / 2.2: Corey-Fuchs reaction;
DOI:10.5012/bkcs.2012.33.6.2055

Reference yield:

: 21573-31-9
oct-7-enal

: 1390635-59-2
C₂₄H₂₅F₃O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: triphenylphosphine / dichloromethane / 0 °C

1.2: -78 - 20 °C

2.1: tetrahydrofuran / -78 - 20 °C

3.1: Lindlar's catalyst; hydrogen / ethyl acetate; cyclohexene / 20 °C

4.1: methyllithium lithium bromide / tetrahydrofuran / 2 h / 0 - 20 °C

4.2: 0.17 h / 0 °C

5.1: Amano Lipase AK / hexane / 16 h / 20 °C / Molecular sieve; Inert atmosphere; Enzymatic reaction

6.1: water; lithium hydroxide / tetrahydrofuran / 5 h / 20 °C

7.1: pyridine / dichloromethane / 20 °C

With pyridine; methyllithium lithium bromide; Amano Lipase AK; Lindlar's catalyst; water; hydrogen; triphenylphosphine; lithium hydroxide; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate; cyclohexene; 1.1: Corey-Fuchs reaction / 1.2: Corey-Fuchs reaction;
DOI:10.5012/bkcs.2012.33.6.2055