HPh₂GeGePh₂GePh₂GePh₃

Base Information

• Chemical Name: HPh₂GeGePh₂GePh₂GePh₃
• CAS No.: 1380095-29-3
• Molecular Formula: C₅₄H₄₆Ge₄
• Molecular Weight: 985.319
• Mol file: 1380095-29-3.mol

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Chemical Property of HPh₂GeGePh₂GePh₂GePh₃

Chemical Property:

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Technology Process of HPh₂GeGePh₂GePh₂GePh₃

There total 1 articles about HPh₂GeGePh₂GePh₂GePh₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1,1,2,2,3,3-hexaphenyltrigermane (120154-44-1) + N,N-dimethyltriphenylgermylamine → HPh2GeGePh2GePh2GePh3 (1380095-29-3)

Guidance literature:

In acetonitrile; to soln. HPh2GeGePh2GePh2H in MeCN soln. Ph3GeNMe2 in MeCN was added, heated in sealed Schlenk tube at 85°C for 48 h; volatiles were removed in vacuo; elem. anal.;

DOI:10.1021/om300385n

Reference yield: 83.0%

HPh2GeGePh2GePh2GePh3 (1380095-29-3) + N,N-dimethyltriphenylgermylamine → dodecaphenyl-n-pentagermane

Guidance literature:

In acetonitrile; to soln. Ph3GeGePh2GePh2GePh2H in MeCN soln. Ph3GeNMe2 in MeCN was added, heated in sealed Schlenk tube at 85°C for 48 h; volatiles were removed in vacuo; elem. anal.;

DOI:10.1021/om300385n

upstream raw materials:

1,1,2,2,3,3-hexaphenyltrigermane