Technology Process of N-(3,4-dimethoxyphenethyl)-2,3-methylenedioxyphenylacetamide
There total 2 articles about N-(3,4-dimethoxyphenethyl)-2,3-methylenedioxyphenylacetamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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at 180 ℃;
for 3h;
- Guidance literature:
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Multi-step reaction with 2 steps
1: 97 percent / KOH / H2O; ethanol / 3 h / Heating
2: 90 percent / 3 h / 180 °C
With
potassium hydroxide;
In
ethanol; water;
- Guidance literature:
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Multi-step reaction with 10 steps
1: phosphorus oxychloride / benzene / 3 h / Heating
2: 11.2 g / sodium borohydride / methanol / 2 h / Ambient temperature
3: 63 percent / acetic acid; H2O / 3.5 h / Heating
4: 10.4 g / I2/AcOK / ethanol / 2 h / Heating
5: 97 percent / LAH / tetrahydrofuran / 2 h / Ambient temperature
6: 69 percent / m-CPBA / CH2Cl2 / 1.) -30 deg C, 1 h; 2.) room temp., 1 h
7: 45 percent / methanol / 0.83 h / Ambient temperature; Irradiation
8: 65 percent / benzene / 2 h / 50 °C
9: 90 percent / H2 / 5percent Pd-C / ethanol / Ambient temperature
10: 73 percent / LAH / tetrahydrofuran / 2.5 h / Heating
With
sodium tetrahydroborate; lithium aluminium tetrahydride; hydrogen; iodine; potassium acetate; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid; benzene;