(1,2-Phenylene)bis[chloro(dimethyl)silane]

Base Information

Chemical Name:(1,2-Phenylene)bis[chloro(dimethyl)silane]
CAS No.:109756-03-8
Molecular Formula:C10H16Cl2Si2
Molecular Weight:263.314
Hs Code.:
DSSTox Substance ID:DTXSID60552732
Nikkaji Number:J1.095.824E
Wikidata:Q82433099

Synonyms:109756-03-8;SCHEMBL1459198;phenylenebis[chlorodimethylsilane];DTXSID60552732;(1,2-Phenylene)bis[chloro(dimethyl)silane]

Suppliers and Price of (1,2-Phenylene)bis[chloro(dimethyl)silane]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1,2-Phenylene)bis[chloro(dimethyl)silane]

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:262.0167590
Heavy Atom Count:14
Complexity:182

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C1=CC=CC=C1[Si](C)(C)Cl)Cl

Technology Process of (1,2-Phenylene)bis[chloro(dimethyl)silane]

There total 2 articles about (1,2-Phenylene)bis[chloro(dimethyl)silane] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 17985-72-7
1,2-bis(dimethylsilyl)benzene

: 109756-03-8
1,2-bis(dimethylchlorosilyl)benzene

Guidance literature:: With chlorine; In tetrachloromethane; at 0 ℃;
DOI:10.1016/0022-328X(86)80202-9

Reference yield:

: 583-53-9
2,3-dibromobenzene

: 109756-03-8
1,2-bis(dimethylchlorosilyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / tetrahydrofuran / Inert atmosphere; Schlenk technique

1.2: 3 h / Reflux; Inert atmosphere; Schlenk technique

2.1: palladium dichloride / tetrachloromethane / 3 h / Reflux; Schlenk technique; Inert atmosphere

With magnesium; palladium dichloride; In tetrahydrofuran; tetrachloromethane;
DOI:10.1016/j.jorganchem.2017.11.010