(E)-N-hexadecyl-4-(2-(4-(dimethylamino)phenyl)ethylene)pyridinium tetrakis(1-phenyl-3-methyl-4-benzoyl-5-pyrazolonato)ytterbium(III)

Base Information

Chemical Name:(E)-N-hexadecyl-4-(2-(4-(dimethylamino)phenyl)ethylene)pyridinium tetrakis(1-phenyl-3-methyl-4-benzoyl-5-pyrazolonato)ytterbium(III)
CAS No.:158595-45-0
Molecular Formula:C₃₁H₄₉N₂*C₆₈H₅₂N₈O₈Yb
Molecular Weight:1731.99
Hs Code.:

(E)-N-hexadecyl-4-(2-(4-(dimethylamino)phenyl)ethylene)pyridinium tetrakis(1-phenyl-3-methyl-4-benzoyl-5-pyrazolonato)ytterbium(III)

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Chemical Property of (E)-N-hexadecyl-4-(2-(4-(dimethylamino)phenyl)ethylene)pyridinium tetrakis(1-phenyl-3-methyl-4-benzoyl-5-pyrazolonato)ytterbium(III)

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Technology Process of (E)-N-hexadecyl-4-(2-(4-(dimethylamino)phenyl)ethylene)pyridinium tetrakis(1-phenyl-3-methyl-4-benzoyl-5-pyrazolonato)ytterbium(III)

There total 2 articles about (E)-N-hexadecyl-4-(2-(4-(dimethylamino)phenyl)ethylene)pyridinium tetrakis(1-phenyl-3-methyl-4-benzoyl-5-pyrazolonato)ytterbium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 18923-27-8
ytterbium(III) ion

: 117154-25-3,124730-59-2
(E)-N-n-hexadecyl-4-(2-(4-(dimethylamino)phenyl)ethenyl)pyridinium bromide

: 4551-69-3
4-benzoyl-1-phenyl-3-methyl-2-pyrazolin-5-one

: 158595-45-0
(E)-N-hexadecyl-4-(2-(4-(dimethylamino)phenyl)ethylene)pyridinium tetrakis(1-phenyl-3-methyl-4-benzoyl-5-pyrazolonato)ytterbium(III)

Guidance literature:: With NaOH; In ethanol; β-diketone deprotonated with equiv. amount of NaOH; 4 equiv. of β-diketone reacted with Br-compound and rare earth compound (4:1:1 molar ratio) in EtOH; for the rare earth compound either the hydrated nitrate or the chloride salt is used; recrystallized from EtOH/water 1:1 mixt.; elem. anal.;
DOI:10.1016/j.poly.2007.08.005

Reference yield:

: 117154-25-3,124730-59-2
(E)-N-n-hexadecyl-4-(2-(4-(dimethylamino)phenyl)ethenyl)pyridinium bromide

: ytterbium(III) nitrate

: 4551-69-3
4-benzoyl-1-phenyl-3-methyl-2-pyrazolin-5-one

: 158595-45-0
(E)-N-hexadecyl-4-(2-(4-(dimethylamino)phenyl)ethylene)pyridinium tetrakis(1-phenyl-3-methyl-4-benzoyl-5-pyrazolonato)ytterbium(III)

Guidance literature:: In ethanol; water; neutralized (aq. NaOH), vigorous stirring, reflux (water bath, 0.5 h); filtn., recrystn.; elem. anal.;
DOI:10.1021/j100039a029