(S)-2-Acetylamino-N-[3-(4-{3-[(S)-2-acetylamino-3-(4-hydroxy-phenyl)-propionylamino]-propylamino}-butylamino)-propyl]-3-(4-hydroxy-phenyl)-propionamide

Base Information

Chemical Name:(S)-2-Acetylamino-N-[3-(4-{3-[(S)-2-acetylamino-3-(4-hydroxy-phenyl)-propionylamino]-propylamino}-butylamino)-propyl]-3-(4-hydroxy-phenyl)-propionamide
CAS No.:132087-53-7
Molecular Formula:C₃₂H₄₈N₆O₆
Molecular Weight:612.77
Hs Code.:

(S)-2-Acetylamino-N-[3-(4-{3-[(S)-2-acetylamino-3-(4-hydroxy-phenyl)-propionylamino]-propylamino}-butylamino)-propyl]-3-(4-hydroxy-phenyl)-propionamide

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-Acetylamino-N-[3-(4-{3-[(S)-2-acetylamino-3-(4-hydroxy-phenyl)-propionylamino]-propylamino}-butylamino)-propyl]-3-(4-hydroxy-phenyl)-propionamide

Chemical Property:

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Technology Process of (S)-2-Acetylamino-N-[3-(4-{3-[(S)-2-acetylamino-3-(4-hydroxy-phenyl)-propionylamino]-propylamino}-butylamino)-propyl]-3-(4-hydroxy-phenyl)-propionamide

There total 5 articles about (S)-2-Acetylamino-N-[3-(4-{3-[(S)-2-acetylamino-3-(4-hydroxy-phenyl)-propionylamino]-propylamino}-butylamino)-propyl]-3-(4-hydroxy-phenyl)-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-2-Acetylamino-N-[3-(4-{3-[(S)-2-acetylamino-3-(4-benzyloxy-phenyl)-propionylamino]-propylamino}-butylamino)-propyl]-3-(4-benzyloxy-phenyl)-propionamide

: 132087-53-7
(S)-2-Acetylamino-N-[3-(4-{3-[(S)-2-acetylamino-3-(4-hydroxy-phenyl)-propionylamino]-propylamino}-butylamino)-propyl]-3-(4-hydroxy-phenyl)-propionamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1016/S0040-4020(01)85463-6

Reference yield:

: 2130-96-3,54784-43-9
O-benzyl-N-tert-butoxycarbonyl-L-tyrosine

: 132087-53-7
(S)-2-Acetylamino-N-[3-(4-{3-[(S)-2-acetylamino-3-(4-hydroxy-phenyl)-propionylamino]-propylamino}-butylamino)-propyl]-3-(4-hydroxy-phenyl)-propionamide

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / dicyclohexylcarbodiimide / ethyl acetate / 1.5 h / Ambient temperature

2: CF₃CO₂H / CHCl₃ / 2 h / Ambient temperature

3: Et₃N / CHCl₃ / Ambient temperature

4: methanol / Ambient temperature

5: H₂ / 5percent Pd/C / methanol

With hydrogen; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium on activated charcoal; In methanol; chloroform; ethyl acetate;
DOI:10.1016/S0040-4020(01)85463-6

Reference yield:

: 13512-59-9
N-(tert-butyloxycarbonyl)-O-(phenylmethyl)-L-tyrosine 4-nitrophenol ester

: 132087-53-7
(S)-2-Acetylamino-N-[3-(4-{3-[(S)-2-acetylamino-3-(4-hydroxy-phenyl)-propionylamino]-propylamino}-butylamino)-propyl]-3-(4-hydroxy-phenyl)-propionamide

Guidance literature:: Multi-step reaction with 4 steps

1: CF₃CO₂H / CHCl₃ / 2 h / Ambient temperature

2: Et₃N / CHCl₃ / Ambient temperature

3: methanol / Ambient temperature

4: H₂ / 5percent Pd/C / methanol

With hydrogen; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1016/S0040-4020(01)85463-6