Technology Process of C33H42FN3O5
There total 4 articles about C33H42FN3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,1'-carbonyldiimidazole;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 2h;
DOI:10.1016/j.bmcl.2010.11.103
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 0.5 h / 0 °C
2: toluene-4-sulfonic acid; acetic acid / 5,5-dimethyl-1,3-cyclohexadiene / 16 h / Reflux
3: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 25 °C
4: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C
With
palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; acetic acid; triethylamine; 1,1'-carbonyldiimidazole;
In
methanol; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.11.103
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid; acetic acid / 5,5-dimethyl-1,3-cyclohexadiene / 16 h / Reflux
2: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 25 °C
3: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C
With
palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; acetic acid; 1,1'-carbonyldiimidazole;
In
methanol; 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.11.103
