CHO₂^(1-)*C₁₈H₃₁N₂O₄S⁽¹⁺⁾

Base Information

• Chemical Name: CHO₂^(1-)*C₁₈H₃₁N₂O₄S⁽¹⁺⁾
• CAS No.: 1226913-83-2
• Molecular Formula: CHO₂*C₁₈H₃₁N₂O₄S
• Molecular Weight: 416.539
• Mol file: 1226913-83-2.mol

Synonyms:

Chemical Property of CHO₂^(1-)*C₁₈H₃₁N₂O₄S⁽¹⁺⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of CHO₂^(1-)*C₁₈H₃₁N₂O₄S⁽¹⁺⁾

There total 8 articles about CHO₂^(1-)*C₁₈H₃₁N₂O₄S⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H21NO5S (1123693-96-8) → CHO2(1-)*C18H31N2O4S(1+) (1226913-83-2)

Guidance literature:

Multi-step reaction with 4 steps

1: N,N-dimethyl-formamide / 16 h / 20 - 70 °C

2: methanol; sodium hydroxide / water / 1 h

3: caesium carbonate / water; N,N-dimethyl-formamide / 16 h / 20 °C

4: formic acid; dihydrogen peroxide / 2 h / 20 °C

With methanol; formic acid; dihydrogen peroxide; caesium carbonate; sodium hydroxide; In water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2011.04.084

Reference yield:

benzyl 4-mercapto-2-methylbutan-2-ylcarbamate (1226913-81-0) → CHO2(1-)*C18H31N2O4S(1+) (1226913-83-2)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate / water; N,N-dimethyl-formamide / 16 h / 20 °C

2: formic acid; dihydrogen peroxide / 2 h / 20 °C

With formic acid; dihydrogen peroxide; caesium carbonate; In water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2011.04.084

Reference yield:

Br(1-)*C18H31N2O2S(1+) (1226913-80-9) → CHO2(1-)*C18H31N2O4S(1+) (1226913-83-2)

Guidance literature:

With formic acid; dihydrogen peroxide; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2011.04.084

upstream raw materials:

C₁₄H₂₁NO₅S

benzyl 4-mercapto-2-methylbutan-2-ylcarbamate

Br^(1-)*C₁₈H₃₁N₂O₂S⁽¹⁺⁾

3-Methylbutenoic acid