[(AuPPh3)2(μ-NH2)]ClO4

Base Information

Chemical Name:[(AuPPh3)2(μ-NH2)]ClO4
CAS No.:194206-77-4
Molecular Formula:C₃₆H₃₂Au₂NP₂*ClO₄
Molecular Weight:1033.99
Hs Code.:

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Chemical Property of [(AuPPh3)2(μ-NH2)]ClO4

Chemical Property:

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Technology Process of [(AuPPh3)2(μ-NH2)]ClO4

There total 3 articles about [(AuPPh3)2(μ-NH2)]ClO4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3-[(triphenylphosphine)gold]pentane-2,4-dione

: 194206-63-8
Au(NH₃)(P(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)=[Au(NH₃)(P(C₆H₅)3)]ClO₄

: 194206-77-4
[(AuPPh3)2(μ-NH2)]ClO4

Guidance literature:: In dichloromethane; byproducts: acetylacetone; N2-atmosphere; stirring at room temp. for 10 min; concn., pptn. on Et2O addn., recrystn. (CH2Cl2 and Et2O); elem. anal.;
DOI:10.1021/ic970225j

Reference yield:

: 3-[(triphenylphosphine)gold]pentane-2,4-dione

: 194206-77-4
[(AuPPh3)2(μ-NH2)]ClO4

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: dichloromethane

In tetrahydrofuran; dichloromethane;
DOI:10.1021/ic970225j

Reference yield:

: 3-[(triphenylphosphine)gold]pentane-2,4-dione

: 194206-63-8
Au(NH₃)(P(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)=[Au(NH₃)(P(C₆H₅)3)]ClO₄

: 7732-18-5
water

: [(AuPPh3)3(μ-O)]ClO4

: 194206-77-4
[(AuPPh3)2(μ-NH2)]ClO4

Guidance literature:: In dichloromethane; byproducts: acetylacetone; N2-atmosphere; stirring at room temp. (source of water unclear);
DOI:10.1021/ic970225j