Pt(CCCH₂CH₂C₆H₅)2(P(C₆H₅)2CH₂P(C₆H₅)2)2

Base Information

Chemical Name:Pt(CCCH₂CH₂C₆H₅)2(P(C₆H₅)2CH₂P(C₆H₅)2)2
CAS No.:88762-38-3
Molecular Formula:C₇₀H₆₂P₄Pt
Molecular Weight:1222.24
Hs Code.:

Pt(CCCH<sub>2</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)2(P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2

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Chemical Property of Pt(CCCH₂CH₂C₆H₅)2(P(C₆H₅)2CH₂P(C₆H₅)2)2

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Technology Process of Pt(CCCH₂CH₂C₆H₅)2(P(C₆H₅)2CH₂P(C₆H₅)2)2

There total 1 articles about Pt(CCCH₂CH₂C₆H₅)2(P(C₆H₅)2CH₂P(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 52595-94-5
PtCl₂(dppm)

: 4-phenyl-1-butynyllithium

: 2071-20-7
bis-diphenylphosphinomethane

: 88762-38-3
Pt(CCCH₂CH₂C₆H₅)2(P(C₆H₅)2CH₂P(C₆H₅)2)2

Guidance literature:: In hexane; benzene; a soln. of Pt-complex and dppm (1 mole-equivalent) in C6H6 was added toa soln. of ligand (2 mole-equivalent) in hexane, refluxed for 1.5 h, cooled, stirred for 14 h at 20°C; evapd., recrystd. from C6H6-MeOH; elem. anal.;

Reference yield: 89.0%

: 4Ag⁽¹⁺⁾*4Cl^(1-)*4P(C₆H₅)3 = [Ag₄Cl₄(P(C₆H₅)3)4]

: 88762-38-3
Pt(CCCH₂CH₂C₆H₅)2(P(C₆H₅)2CH₂P(C₆H₅)2)2

: (C₆H₅CH₂CH₂CC)2Pt(P(C₆H₅)2CH₂P(C₆H₅)2)2AgCl

Guidance literature:: In dichloromethane; Ag-complex was added to soln. of Pt-complex in CH2Cl2, Et2O was added, soln. was reduced in vol., Et2O was added; mixt. was reduced, ppt. was filtered off, washed with Et2O, dried in vac.; elem. anal.;
DOI:10.1039/DT9840000855

Reference yield: 76.0%

: 14877-90-8,16970-35-7
trans-chlorocarbonylbis(triphenylarsine)rhodium(I)

: 88762-38-3
Pt(CCCH₂CH₂C₆H₅)2(P(C₆H₅)2CH₂P(C₆H₅)2)2

: 100908-49-4
C₆H₅CH₂CH₂C₂Pt(P(C₆H₅)2CH₂P(C₆H₅)2)2C₂C₆H₅CH₂CH₂RhCO⁽¹⁺⁾*Cl^(1-)=(C₂C₆H₅CH₂CH₂)Pt(P(C₆H₅)2CH₂P(C₆H₅)2)2C₂C₆H₅CH₂CH₂RhCOCl

Guidance literature:: In benzene; a soln. of Rh-complex in benzene was added to a soln. of Pt-complex in warm benzene, cooled to ca. 20°C; sepd., filtered, washed with benzene, dried in vac.;
DOI:10.1039/DT9850002121