C₂₆H₃₁ClO₆

Base Information

• Chemical Name: C₂₆H₃₁ClO₆
• CAS No.: 1609477-62-4
• Molecular Formula: C₂₆H₃₁ClO₆
• Molecular Weight: 474.982
• Mol file: 1609477-62-4.mol

Synonyms:

Chemical Property of C₂₆H₃₁ClO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₃₁ClO₆

There total 4 articles about C₂₆H₃₁ClO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 4-hydroxy-3-chlorobenzoate (3964-57-6) → C26H31ClO6 (1609477-62-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 6 h / 85 °C / Inert atmosphere

2: potassium carbonate; potassium iodide / acetonitrile / 0.25 h / 160 °C / Inert atmosphere; Microwave irradiation

With potassium carbonate; potassium iodide; In acetonitrile;

DOI:10.1021/jm5000563

Reference yield:

2-cyclopentylacetic acid (1123-00-8) → C26H31ClO6 (1609477-62-4)

Guidance literature:

Multi-step reaction with 3 steps

1: oxalyl dichloride / dichloromethane

2: aluminum (III) chloride / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

3: potassium carbonate; potassium iodide / acetonitrile / 0.25 h / 160 °C / Inert atmosphere; Microwave irradiation

With aluminum (III) chloride; oxalyl dichloride; potassium carbonate; potassium iodide; In dichloromethane; acetonitrile; 2: |Friedel-Crafts Acylation;

DOI:10.1021/jm5000563

Reference yield:

2-cyclopentylacetyl chloride (1122-99-2) → C26H31ClO6 (1609477-62-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate; potassium iodide / acetonitrile / 0.25 h / 160 °C / Inert atmosphere; Microwave irradiation

With aluminum (III) chloride; potassium carbonate; potassium iodide; In dichloromethane; acetonitrile; 1: |Friedel-Crafts Acylation;

DOI:10.1021/jm5000563

upstream raw materials:

methyl 4-hydroxy-3-chlorobenzoate

2-cyclopentylacetic acid

2-cyclopentylacetyl chloride

2-methylbenzene-1,3-diol

Downstream raw materials:

3-chloro-4-{4-[4-(2-cyclopentylacetyl)-3-hydroxy-2-methylphenoxy]butoxy}benzoic acid