C₁₈H₁₈O₄

Base Information

Chemical Name:C₁₈H₁₈O₄
CAS No.:1431381-25-7
Molecular Formula:C₁₈H₁₈O₄
Molecular Weight:298.339
Hs Code.:

C<sub>18</sub>H<sub>18</sub>O<sub>4</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₈O₄

Chemical Property:

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Technology Process of C₁₈H₁₈O₄

There total 3 articles about C₁₈H₁₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 2475-14-1
6-methyl-1-phenylhepta-2,4-diyne-1,6-diol

: 108-24-7
acetic anhydride

: 1431381-25-7
C₁₈H₁₈O₄

Guidance literature:: With copper(II) choride dihydrate; palladium dichloride; at 60 ℃; Schlenk technique;
DOI:10.1021/jo400276e

Reference yield:

: 2063-19-6
4-bromo-2-methylbut-3-yn-2-ol

: 1431381-25-7
C₁₈H₁₈O₄

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) chloride; N-butylamine; hydroxylamine hydrochloride / water; diethyl ether / 0 °C

2: palladium dichloride; copper(II) choride dihydrate / 60 °C / Schlenk technique

With copper(II) choride dihydrate; hydroxylamine hydrochloride; N-butylamine; copper(l) chloride; palladium dichloride; In diethyl ether; water;
DOI:10.1021/jo400276e

Reference yield:

: 115-19-5
2-methyl-but-3-yn-2-ol

: 1431381-25-7
C₁₈H₁₈O₄

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; silver nitrate / acetone / 3 h / 20 °C

2: copper(l) chloride; N-butylamine; hydroxylamine hydrochloride / water; diethyl ether / 0 °C

3: palladium dichloride; copper(II) choride dihydrate / 60 °C / Schlenk technique

With N-Bromosuccinimide; copper(II) choride dihydrate; hydroxylamine hydrochloride; silver nitrate; N-butylamine; copper(l) chloride; palladium dichloride; In diethyl ether; water; acetone;
DOI:10.1021/jo400276e