[1R-[1α(R*),3aβ,3bα,5aβ,12aα,12bβ,14aα]]-1-(1,5-dimethylhexyl)-1,2,3,3a,3b,4,5,11,12,12a,12b,13,14,14a-tetradecahydro-12a,14a-dimethyl-8-propylcyclopenta[5,6]naphtho[2,1-d][1,2,4]triazolo[1,5-a]azepinium picrate

Base Information

Chemical Name:[1R-[1α(R*),3aβ,3bα,5aβ,12aα,12bβ,14aα]]-1-(1,5-dimethylhexyl)-1,2,3,3a,3b,4,5,11,12,12a,12b,13,14,14a-tetradecahydro-12a,14a-dimethyl-8-propylcyclopenta[5,6]naphtho[2,1-d][1,2,4]triazolo[1,5-a]azepinium picrate
CAS No.:1369392-65-3
Molecular Formula:C₆H₃N₃O₇*C₃₁H₅₃N₃
Molecular Weight:696.888
Hs Code.:

[1R-[1α(R*),3aβ,3bα,5aβ,12aα,12bβ,14aα]]-1-(1,5-dimethylhexyl)-1,2,3,3a,3b,4,5,11,12,12a,12b,13,14,14a-tetradecahydro-12a,14a-dimethyl-8-propylcyclopenta[5,6]naphtho[2,1-d][1,2,4]triazolo[1,5-a]azepinium picrate

Synonyms:

Suppliers and Price of [1R-[1α(R*),3aβ,3bα,5aβ,12aα,12bβ,14aα]]-1-(1,5-dimethylhexyl)-1,2,3,3a,3b,4,5,11,12,12a,12b,13,14,14a-tetradecahydro-12a,14a-dimethyl-8-propylcyclopenta[5,6]naphtho[2,1-d][1,2,4]triazolo[1,5-a]azepinium picrate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [1R-[1α(R*),3aβ,3bα,5aβ,12aα,12bβ,14aα]]-1-(1,5-dimethylhexyl)-1,2,3,3a,3b,4,5,11,12,12a,12b,13,14,14a-tetradecahydro-12a,14a-dimethyl-8-propylcyclopenta[5,6]naphtho[2,1-d][1,2,4]triazolo[1,5-a]azepinium picrate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [1R-[1α(R*),3aβ,3bα,5aβ,12aα,12bβ,14aα]]-1-(1,5-dimethylhexyl)-1,2,3,3a,3b,4,5,11,12,12a,12b,13,14,14a-tetradecahydro-12a,14a-dimethyl-8-propylcyclopenta[5,6]naphtho[2,1-d][1,2,4]triazolo[1,5-a]azepinium picrate

There total 5 articles about [1R-[1α(R*),3aβ,3bα,5aβ,12aα,12bβ,14aα]]-1-(1,5-dimethylhexyl)-1,2,3,3a,3b,4,5,11,12,12a,12b,13,14,14a-tetradecahydro-12a,14a-dimethyl-8-propylcyclopenta[5,6]naphtho[2,1-d][1,2,4]triazolo[1,5-a]azepinium picrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1369392-64-2
[1R-[1α(R*),3aβ,3bα,5aβ,12aα,12bβ,14aα]]-1-(1,5-dimethylhexyl)-1,2,3,3a,3b,4,5,11,12,12a,12b,13,14,14a-tetradecahydro-12a,14a-dimethyl-8-phenylcyclopenta[5,6]naphtho[2,1-d][1,2,4]triazolo[1,5-a]azepine

: 88-89-1
2,4,6-Trinitrophenol

: 1369392-65-3
[1R-[1α(R*),3aβ,3bα,5aβ,12aα,12bβ,14aα]]-1-(1,5-dimethylhexyl)-1,2,3,3a,3b,4,5,11,12,12a,12b,13,14,14a-tetradecahydro-12a,14a-dimethyl-8-propylcyclopenta[5,6]naphtho[2,1-d][1,2,4]triazolo[1,5-a]azepinium picrate

Guidance literature:: In methanol;
DOI:10.1016/j.steroids.2012.01.016

Reference yield:

: 1369392-70-0
5α-cholestan-3-one (N-ethoxycarbonyl)hydrazone

: 1369392-65-3
[1R-[1α(R*),3aβ,3bα,5aβ,12aα,12bβ,14aα]]-1-(1,5-dimethylhexyl)-1,2,3,3a,3b,4,5,11,12,12a,12b,13,14,14a-tetradecahydro-12a,14a-dimethyl-8-propylcyclopenta[5,6]naphtho[2,1-d][1,2,4]triazolo[1,5-a]azepinium picrate

Guidance literature:: Multi-step reaction with 6 steps

1: tert-butylhypochlorite / dichloromethane / 0.33 h / 0 °C / Darkness

2: antimonypentachloride / dichloromethane / 0.5 h / -70 - -60 °C / Inert atmosphere

3: antimonypentachloride / dichloromethane / 2 h / -60 - -30 °C / Inert atmosphere

4: dichloromethane / 1.5 h / 30 °C / Inert atmosphere

5: sodium hydroxide / dichloromethane; water / 0.33 h / 0 - 20 °C / Inert atmosphere

6: methanol

With tert-butylhypochlorite; antimonypentachloride; sodium hydroxide; In methanol; dichloromethane; water;
DOI:10.1016/j.steroids.2012.01.016

Reference yield:

: C₃₄H₅₈N₃O₂⁽¹⁺⁾*Cl₆Sb^(1-)

: 1369392-65-3
[1R-[1α(R*),3aβ,3bα,5aβ,12aα,12bβ,14aα]]-1-(1,5-dimethylhexyl)-1,2,3,3a,3b,4,5,11,12,12a,12b,13,14,14a-tetradecahydro-12a,14a-dimethyl-8-propylcyclopenta[5,6]naphtho[2,1-d][1,2,4]triazolo[1,5-a]azepinium picrate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 1.5 h / 30 °C / Inert atmosphere

2: sodium hydroxide / dichloromethane; water / 0.33 h / 0 - 20 °C / Inert atmosphere

3: methanol

With sodium hydroxide; In methanol; dichloromethane; water;
DOI:10.1016/j.steroids.2012.01.016