(3-iodopropyl)triphenylplumbane

Base Information

Chemical Name:(3-iodopropyl)triphenylplumbane
CAS No.:134879-54-2
Molecular Formula:C₂₁H₂₁IPb
Molecular Weight:607.502
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-iodopropyl)triphenylplumbane

Chemical Property:

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Technology Process of (3-iodopropyl)triphenylplumbane

There total 1 articles about (3-iodopropyl)triphenylplumbane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.6%

: 3124-01-4
hexaphenyl diplumbane

: 134879-54-2
(3-iodopropyl)triphenylplumbane

Guidance literature:: With Li; In tetrahydrofuran; (Ar), reacted at 25°C for 45 min., centrifuged, transferred by syringe to second flask, stirred, treated dropwise at 0°C with C3H6I2, stirred at 0°C for 24 h, treated with H2O, stirred briefly at 25°C, treated in air; extracted with CH2Cl2, dried (MgSO4), removed solvent in vac., chromy. (Al2O3, hexane, ethyl acetate), recrystd. from ethanol; elem. anal., NMR;
DOI:10.1021/om00054a069

Reference yield:

: 134879-54-2
(3-iodopropyl)triphenylplumbane

: diiodo(3-iodopropyl)phenylplumbane

Guidance literature:: With I₂; In chloroform-d1; (N2), stirred, treated with 2 equiv I2 at 0°C; NMR;
DOI:10.1021/om00054a069

Reference yield:

: 134879-54-2
(3-iodopropyl)triphenylplumbane

: 134879-58-6
iodo(3-iodopropyl)diphenylplumbane

Guidance literature:: With I₂; In chloroform-d1; byproducts: iodobenzene; (N2), stirred, treated with 1 equiv I2 at 0°C; NMR;
DOI:10.1021/om00054a069