PdI₂{(C₆H₅)2PC₅H₄N}2

Base Information

Chemical Name:PdI₂{(C₆H₅)2PC₅H₄N}2
CAS No.:142037-94-3
Molecular Formula:C₃₄H₂₈I₂N₂P₂Pd
Molecular Weight:886.786
Hs Code.:

PdI<sub>2</sub>{(C<sub>6</sub>H<sub>5</sub>)2PC<sub>5</sub>H<sub>4</sub>N}2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of PdI₂{(C₆H₅)2PC₅H₄N}2

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Technology Process of PdI₂{(C₆H₅)2PC₅H₄N}2

There total 2 articles about PdI₂{(C₆H₅)2PC₅H₄N}2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.2%

: 38255-46-8,84773-43-3,78088-45-6,1246525-11-0
cis-{PdCl₂(PPh₂py-P)2}

: 38255-46-8,84773-43-3,78088-45-6,1246525-11-0
{bis(diphenylphosphino)-2-pyridyl}palladium(II) chloride

: 133483-37-1,142037-94-3
trans-{PdI₂(PPh₂py-P)2}

Guidance literature:: With KI; In not given; elem. anal.;
DOI:10.1246/bcsj.63.3434

Reference yield:

: 38255-46-8,84773-43-3,78088-45-6,1246525-11-0
cis-{PdCl₂(PPh₂py-P)2}

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 133483-37-1,142037-94-3
trans-{PdI₂(PPh₂py-P)2}

Guidance literature:: In methanol; dichloromethane; water; (N2); addn. of 10 equiv. of NaI dissolved in H2O to Pd-compd. in CH2Cl2, addn. of MeOH, stirring at room temp. (2 h); crystn. by redn. of vol., collection, washing (H2O, MeOH), drying in vac.; elem. anal.;

Reference yield: 85.3%

: 52522-40-4
tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex

: 133483-37-1,142037-94-3
PdI₂{(C₆H₅)2PC₅H₄N}2

: Pd₂I₂{(C₆H₅)2PC₅H₄N}2*0.5CH₂Cl₂

Guidance literature:: With dichloromethane; In dichloromethane; heating a mixt. of Pd-compds. for 16 h according to a method of A. Maisonnet, J. P. Farr, M. M. Olmstead, C. T. Hunt, and A. L. Balch, Inorg. Chem. 21, 3961 (1982); filtration in air, evapn. of filtrate, pptn. upon addn. of diethyl ether, recrystn. (CH2Cl2/MeOH 2:1), slow evapn. in a desiccator, filtration, drying in air, elem. anal.;
DOI:10.1246/bcsj.65.1016