palladium 2-formyl-5,10,15,20-tetraphenylporphyrinate

Base Information

Chemical Name:palladium 2-formyl-5,10,15,20-tetraphenylporphyrinate
CAS No.:1015309-47-3
Molecular Formula:C₄₅H₂₈N₄OPd
Molecular Weight:747.164
Hs Code.:

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Chemical Property of palladium 2-formyl-5,10,15,20-tetraphenylporphyrinate

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Technology Process of palladium 2-formyl-5,10,15,20-tetraphenylporphyrinate

There total 1 articles about palladium 2-formyl-5,10,15,20-tetraphenylporphyrinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14187-13-4
palladium(II) tetraphenylporphyrin

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1015309-47-3
palladium 2-formyl-5,10,15,20-tetraphenylporphyrinate

Guidance literature:: With trichlorophosphate; Vilsmeier formylation of palladium compd.;
DOI:10.1007/s11172-007-0026-z

Reference yield: 78.0%

: 1015309-47-3
palladium 2-formyl-5,10,15,20-tetraphenylporphyrinate

: 2065-66-9
methyl-triphenylphosphonium iodide

: 1021328-80-2
palladium 2-vinyl-5,10,15,20-tetraphenylporphyrinate

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In benzene; (Ar); refluxing mixt. of palladium compd., triphenylmethylphosphonium salt, potassium carbonate and 18-crown-6 in anhydrous benzene for 18 h; cooling, filtration through Al2O3, concn., chromy. (silica gel, benzene), evapn., recrystn. (CHCl3-methanol (1:3)), elem. anal.;
DOI:10.1007/s11172-007-0026-z