C₁₃H₂₀O₃

Base Information

Chemical Name:C₁₃H₂₀O₃
CAS No.:625095-90-1
Molecular Formula:C₁₃H₂₀O₃
Molecular Weight:224.3
Hs Code.:

C<sub>13</sub>H<sub>20</sub>O<sub>3</sub>

Synonyms:

Suppliers and Price of C₁₃H₂₀O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₂₀O₃

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₁₃H₂₀O₃

There total 13 articles about C₁₃H₂₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₈O₃

: 625095-90-1
C₁₃H₂₀O₃

Guidance literature:: With sodium tetrahydroborate; In ethanol; water; at 20 ℃; for 0.166667h;
DOI:10.1002/ejoc.201402096

Reference yield:

: 1622095-12-8
C₂₀H₁₉NO₅

: 625095-90-1
C₁₃H₂₀O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: dichloromethane / 20 h / 20 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

2.2: 11.5 h / -78 - -5 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; water / 18 h / 20 °C

4.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 2 h / -78 °C / Inert atmosphere

5.1: dimethylsulfide borane complex / tetrahydrofuran / 9 h / 20 °C / Inert atmosphere; Cooling with ice

5.2: 5 h / 20 °C / Inert atmosphere

6.1: sodium periodate / water; ethanol / 0.33 h / 20 °C

7.1: sodium tetrahydroborate / water; ethanol / 0.17 h / 20 °C

With sodium tetrahydroborate; sodium periodate; dimethylsulfide borane complex; sodium hexamethyldisilazane; diisobutylaluminium hydride; In tetrahydrofuran; ethanol; dichloromethane; cyclohexane; water; 1.1: |Wittig Olefination;
DOI:10.1002/ejoc.201402096

Reference yield:

: 99865-70-0
4-(4-Formyl-phenoxy)butyric acid

: 625095-90-1
C₁₃H₂₀O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 14 h / 20 °C

2.1: dichloromethane / 20 h / 20 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

3.2: 11.5 h / -78 - -5 °C

4.1: sodium tetrahydroborate / tetrahydrofuran; water / 18 h / 20 °C

5.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 2 h / -78 °C / Inert atmosphere

6.1: dimethylsulfide borane complex / tetrahydrofuran / 9 h / 20 °C / Inert atmosphere; Cooling with ice

6.2: 5 h / 20 °C / Inert atmosphere

7.1: sodium periodate / water; ethanol / 0.33 h / 20 °C

8.1: sodium tetrahydroborate / water; ethanol / 0.17 h / 20 °C

With dmap; sodium tetrahydroborate; sodium periodate; dimethylsulfide borane complex; sodium hexamethyldisilazane; diisobutylaluminium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethanol; dichloromethane; cyclohexane; water; 2.1: |Wittig Olefination;
DOI:10.1002/ejoc.201402096