C₁₃H₁₂O₂

Base Information

Chemical Name:C₁₃H₁₂O₂
CAS No.:1437311-48-2
Molecular Formula:C₁₃H₁₂O₂
Molecular Weight:200.237
Hs Code.:

C<sub>13</sub>H<sub>12</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₂O₂

Chemical Property:

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Technology Process of C₁₃H₁₂O₂

There total 5 articles about C₁₃H₁₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(2-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)-3-(trimethylsilyl)prop-2-yn-1-ol

: 1437311-48-2
C₁₃H₁₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.67 h / 0 °C

1.2: 4 h / 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / Reflux

With tetrabutyl ammonium fluoride; sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; ethyl acetate; mineral oil;
DOI:10.1021/ol4011129

Reference yield:

: 1437311-23-3
(2-(1-(allyloxy)prop-2-yn-1-yl)phenyl)methanol

: 1437311-48-2
C₁₃H₁₂O₂

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethyl acetate; for 4h; Reflux;
DOI:10.1021/ol4011129

Reference yield:

: 81168-17-4
2-(tert-butyldimethylsiloxymethyl)benzyl alcohol

: 1437311-48-2
C₁₃H₁₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 1 h / 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.67 h / 0 °C

3.2: 4 h / 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C

5.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / Reflux

With n-butyllithium; tetrabutyl ammonium fluoride; sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; ethyl acetate; mineral oil;
DOI:10.1021/ol4011129