closo-2,3-Ph₂-2,3-C₂B₉H₉

Base Information

• Chemical Name: closo-2,3-Ph₂-2,3-C₂B₉H₉
• CAS No.: 69461-67-2
• Molecular Formula: C₁₄H₁₉B₉
• Molecular Weight: 284.604

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Chemical Property of closo-2,3-Ph₂-2,3-C₂B₉H₉

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Technology Process of closo-2,3-Ph₂-2,3-C₂B₉H₉

There total 1 articles about closo-2,3-Ph₂-2,3-C₂B₉H₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Bu4N)(7,9-Ph2-nido-7,9-C2B8H10) → closo-2,3-Ph2-2,3-C2B9H9 (69461-67-2)

Guidance literature:

With H₂SO₄; In benzene; under N2; stirred and cooled (0°C, ice bath) suspn. of B compd. in benzene treated with concd. H2SO4; heated at 40°C for 1 h; benzene layer sepd.; dried (MgSO4); solvent removed under reduced pressure; sublimed (50°C, 0.1 mmHg);

DOI:10.1039/b203920f

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