[(η3-C5H3Ph2)Pt(PEt3)2]O2CCF3

Base Information

Chemical Name:[(η3-C5H3Ph2)Pt(PEt3)2]O2CCF3
CAS No.:479420-74-1
Molecular Formula:C₂F₃O₂*C₂₉H₄₃P₂Pt
Molecular Weight:761.704
Hs Code.:

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Chemical Property of [(η3-C5H3Ph2)Pt(PEt3)2]O2CCF3

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Technology Process of [(η3-C5H3Ph2)Pt(PEt3)2]O2CCF3

There total 6 articles about [(η3-C5H3Ph2)Pt(PEt3)2]O2CCF3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 479420-70-7,479498-64-1
cis-(Et₃P)2Pt(Me)(Z-CHCH-cyclo-C₃HPh₂)

: 76-05-1
trifluoroacetic acid

: 479420-74-1
[(η3-C5H3Ph2)Pt(PEt3)2]O2CCF3

Guidance literature:: In diethyl ether; inert atm., Schlenk technique; soln. of Pt complex was cooled to -60°C, CF3CO2H was added, soln. was stirred for 10 min at -60°C, then warmed to room tamp. and stirred overnight; ppt. was filtered, washed with Et2O, dried in vac., second crop was obtained from filtrate after additional 24 h of stirring; elem. anal.;
DOI:10.1021/om0206507

Reference yield:

: trans-[Pt(Me)I(PEt₃)2]

: 479420-74-1
[(η3-C5H3Ph2)Pt(PEt3)2]O2CCF3

Guidance literature:: Multi-step reaction with 2 steps

1: BuLi / diethyl ether

2: diethyl ether

With BuLi; In diethyl ether;
DOI:10.1021/om0206507

Reference yield:

: 223248-78-0
(Z)-(3-(2-iodovinyl)cycloprop-1-ene-1,2-diyl)dibenzene

: 479420-74-1
[(η3-C5H3Ph2)Pt(PEt3)2]O2CCF3

Guidance literature:: Multi-step reaction with 2 steps

1: BuLi / diethyl ether

2: diethyl ether

With BuLi; In diethyl ether;
DOI:10.1021/om0206507