boron difluoride p-(α-bromoethyl)benzoylacetonate

Base Information

• Chemical Name: boron difluoride p-(α-bromoethyl)benzoylacetonate
• CAS No.: 750626-54-1
• Molecular Formula: C₁₂H₁₂BBrF₂O₂
• Molecular Weight: 316.938

Synonyms:

Chemical Property of boron difluoride p-(α-bromoethyl)benzoylacetonate

Chemical Property:

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Technology Process of boron difluoride p-(α-bromoethyl)benzoylacetonate

There total 1 articles about boron difluoride p-(α-bromoethyl)benzoylacetonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

N-Bromosuccinimide (128-08-5) + boron difluoride p-ethylbenzoylacetonate → boron difluoride p-(α-bromoethyl)benzoylacetonate (750626-54-1)

Guidance literature:

With dibenzoyl peroxide; In tetrachloromethane; mixt. of B compd., N-bromosuccinimide (molar ratio 1:1.3), benzoyl peroxide and anhyd. CCl4 refluxed with stirring for 30 min; quickly cooled to0°C; filtered; filtrate reduced by half; diluted with petroleum ether; storedat 10°C overnight; filtered; ppt. dried in air; elem. anal.;

DOI:10.1023/B:RUGC.0000016026.56938.f2

upstream raw materials:

N-Bromosuccinimide

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