Technology Process of IrH2(P(OCH2)3CC2H5)(C6H5P(CH2CH2CH2P(C6H11)2)2)(1+)*BF4(1-)={IrH2(P(OCH2)3CC2H5)(C6H5P((CH2)3P(C6H11)2)2)}{BF4}
There total 1 articles about IrH2(P(OCH2)3CC2H5)(C6H5P(CH2CH2CH2P(C6H11)2)2)(1+)*BF4(1-)={IrH2(P(OCH2)3CC2H5)(C6H5P((CH2)3P(C6H11)2)2)}{BF4} which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
tetrahydrofuran;
byproducts: TlCl; nitrogen atmosphere; Tl-salt and ligand added to a soln. of the Ir complex; stirring (3 h); addn. of acetone, filtration, filtrate evapd. (vac.); residue washed (water), recrystd. (acetone/ether); isomer ratio syn:anti = 2:1; elem. anal.;