[Ru(C-p-C₆H₄Me)(P(cyclohexyl)3)2(triflate)]

Base Information

Chemical Name:[Ru(C-p-C₆H₄Me)(P(cyclohexyl)3)2(triflate)]
CAS No.:872371-78-3
Molecular Formula:C₄₅H₇₃F₃O₃P₂RuS
Molecular Weight:914.152
Hs Code.:

[Ru(C-p-C<sub>6</sub>H<sub>4</sub>Me)(P(cyclohexyl)3)2(triflate)]

Synonyms:

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Chemical Property of [Ru(C-p-C₆H₄Me)(P(cyclohexyl)3)2(triflate)]

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Technology Process of [Ru(C-p-C₆H₄Me)(P(cyclohexyl)3)2(triflate)]

There total 1 articles about [Ru(C-p-C₆H₄Me)(P(cyclohexyl)3)2(triflate)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872371-73-8
[Ru(C-p-C₆H₄Me)(P(cyclohexyl)3)2Cl]

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 872371-78-3
Ru(CC₆H₄CH₃)(OSO₂CF₃)(P(C₆H₁₁)3)2

Guidance literature:: In benzene-d6; treatment of the soln. of complex in THF with (CH3)3SiOSO2CF3;
DOI:10.1021/om0508482

Reference yield: 64.2%

: 872371-78-3
[Ru(C-p-C₆H₄Me)(P(cyclohexyl)3)2(triflate)]

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 936322-44-0
[Ru(C-p-C₆H₄Me)(P(cyclohexyl)3)2I₂](triflate)

Guidance literature:: In tetrahydrofuran; under N2, Schlenk technique; soln. of I2 (1 equiv.) in THF added to soln. of Ru complex in THF under stirring; mixt. stirred for 1 h; evapd. under vac.; pentane added to residue; suspn. stirred for 10 min; solid filtered and washed with C6H6 and pentane; dried under vac. for 3 h;
DOI:10.1021/om061192v