methyl barbatolate

Base Information

Chemical Name:methyl barbatolate
CAS No.:6161-74-6
Molecular Formula:C₁₉H₁₆O₁₀
Molecular Weight:404.33
Hs Code.:

Synonyms:

Suppliers and Price of methyl barbatolate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl barbatolate

Chemical Property:

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Technology Process of methyl barbatolate

There total 9 articles about methyl barbatolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 114973-09-0
methyl 6-bromomethyl-3-formyl-2,4-dihydroxybenzoate

: 114973-10-3
potassium haematommate

: 6161-74-6
methyl barbatolate

Guidance literature:: In N,N-dimethyl acetamide; for 12h; Ambient temperature;

Reference yield:

: 705-76-0
3,5-dimethoxybenzyl alcohol

: 6161-74-6
methyl barbatolate

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) sodium hydride / 1.) dimethyl sulfoxide, 1 h, 2.) dimethyl sulfoxide, RT, 1 h

2: 1.) phenyllithium / 1.) ether, RT, 24 h, 2.) ether, RT, 1.5 h

3: 78 percent / N-bromosuccinimide / CHCl₃; CCl₄ / 1.) 0 deg C, 1 h, 2.) RT, 2 h

4: 81 percent / methoxymethyltriphenylphosphonium chloride, NaOMe / 1 h / Ambient temperature

5: 1.) phenyllithium / 1.) ether, RT, 24 h, 2.) ether, a) -78 deg C, 1 h, b) from - 78 deg C to RT, 1 h

6: 80 percent / diethyl ether / 0.03 h

7: 42 percent / boron tribromide / 1.) -78 deg C, 0.5 h, 2.) RT, 0.5 h

8: 20 percent / N,N-dimethyl-acetamide / 12 h / Ambient temperature

With N-Bromosuccinimide; sodium methylate; (methoxymethyl)triphenylphosphonium chloride; boron tribromide; sodium hydride; phenyllithium; In tetrachloromethane; diethyl ether; chloroform; N,N-dimethyl acetamide;

Reference yield:

: 73569-69-4
1-methylmethoxy-3,5-dimethoxybenzene

: 6161-74-6
methyl barbatolate

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) phenyllithium / 1.) ether, RT, 24 h, 2.) ether, RT, 1.5 h

2: 78 percent / N-bromosuccinimide / CHCl₃; CCl₄ / 1.) 0 deg C, 1 h, 2.) RT, 2 h

3: 81 percent / methoxymethyltriphenylphosphonium chloride, NaOMe / 1 h / Ambient temperature

4: 1.) phenyllithium / 1.) ether, RT, 24 h, 2.) ether, a) -78 deg C, 1 h, b) from - 78 deg C to RT, 1 h

5: 80 percent / diethyl ether / 0.03 h

6: 42 percent / boron tribromide / 1.) -78 deg C, 0.5 h, 2.) RT, 0.5 h

7: 20 percent / N,N-dimethyl-acetamide / 12 h / Ambient temperature

With N-Bromosuccinimide; sodium methylate; (methoxymethyl)triphenylphosphonium chloride; boron tribromide; phenyllithium; In tetrachloromethane; diethyl ether; chloroform; N,N-dimethyl acetamide;