(2E,4E,6E,8E,10E,12E,14E)-17-((S)-3,4-Dihydroxy-2,6,6-trimethyl-cyclohex-1-enyl)-2,6,11,15-tetramethyl-heptadeca-2,4,6,8,10,12,14-heptaen-16-ynal

Base Information

Chemical Name:(2E,4E,6E,8E,10E,12E,14E)-17-((S)-3,4-Dihydroxy-2,6,6-trimethyl-cyclohex-1-enyl)-2,6,11,15-tetramethyl-heptadeca-2,4,6,8,10,12,14-heptaen-16-ynal
CAS No.:199921-97-6
Molecular Formula:C₃₀H₃₈O₃
Molecular Weight:446.63
Hs Code.:

(2E,4E,6E,8E,10E,12E,14E)-17-((S)-3,4-Dihydroxy-2,6,6-trimethyl-cyclohex-1-enyl)-2,6,11,15-tetramethyl-heptadeca-2,4,6,8,10,12,14-heptaen-16-ynal

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Chemical Property of (2E,4E,6E,8E,10E,12E,14E)-17-((S)-3,4-Dihydroxy-2,6,6-trimethyl-cyclohex-1-enyl)-2,6,11,15-tetramethyl-heptadeca-2,4,6,8,10,12,14-heptaen-16-ynal

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Technology Process of (2E,4E,6E,8E,10E,12E,14E)-17-((S)-3,4-Dihydroxy-2,6,6-trimethyl-cyclohex-1-enyl)-2,6,11,15-tetramethyl-heptadeca-2,4,6,8,10,12,14-heptaen-16-ynal

There total 3 articles about (2E,4E,6E,8E,10E,12E,14E)-17-((S)-3,4-Dihydroxy-2,6,6-trimethyl-cyclohex-1-enyl)-2,6,11,15-tetramethyl-heptadeca-2,4,6,8,10,12,14-heptaen-16-ynal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-6-((3E,5E,7E,9E,11E,13E,15E)-17,17-Dimethoxy-3,7,12,16-tetramethyl-heptadeca-3,5,7,9,11,13,15-heptaen-1-ynyl)-2,2,5,5,7-pentamethyl-3a,4,5,7a-tetrahydro-benzo[1,3]dioxole

: 199921-97-6
(2E,4E,6E,8E,10E,12E,14E)-17-((S)-3,4-Dihydroxy-2,6,6-trimethyl-cyclohex-1-enyl)-2,6,11,15-tetramethyl-heptadeca-2,4,6,8,10,12,14-heptaen-16-ynal

Guidance literature:: With acetic acid; at 20 ℃; for 3h; Yield given;
DOI:10.3891/acta.chem.scand.51-1201

Reference yield:

: ((E)-4,4-Dimethoxy-3-methyl-but-2-enyl)-triphenyl-phosphonium; bromide

: 199921-97-6
(2E,4E,6E,8E,10E,12E,14E)-17-((S)-3,4-Dihydroxy-2,6,6-trimethyl-cyclohex-1-enyl)-2,6,11,15-tetramethyl-heptadeca-2,4,6,8,10,12,14-heptaen-16-ynal

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / CH₂Cl₂ / 42 h / 20 °C

2: 75percent aq AcOH / 3 h / 20 °C

With sodium hydride; acetic acid; In dichloromethane;
DOI:10.3891/acta.chem.scand.51-1201

Reference yield:

: (2E,4E,6E,8E,10E)-2,7,11-Trimethyl-13-((S)-2,2,4,6,6-pentamethyl-3a,6,7,7a-tetrahydro-benzo[1,3]dioxol-5-yl)-trideca-2,4,6,8,10-pentaen-12-ynal

: 199921-97-6
(2E,4E,6E,8E,10E,12E,14E)-17-((S)-3,4-Dihydroxy-2,6,6-trimethyl-cyclohex-1-enyl)-2,6,11,15-tetramethyl-heptadeca-2,4,6,8,10,12,14-heptaen-16-ynal

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / CH₂Cl₂ / 42 h / 20 °C

2: 75percent aq AcOH / 3 h / 20 °C

With sodium hydride; acetic acid; In dichloromethane;
DOI:10.3891/acta.chem.scand.51-1201