Technology Process of C77H101N3O12
There total 11 articles about C77H101N3O12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene / 12 h / Reflux
2: sodium tetrahydroborate / methanol / 4 h
3: dmap / dichloromethane / 20 °C
4: 10% palladium on activated charcoal; hydrogen / 6 h
5: potassium carbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
With
dmap; sodium tetrahydroborate; 10% palladium on activated charcoal; hydrogen; potassium carbonate;
In
methanol; dichloromethane; toluene; acetonitrile;
DOI:10.1002/chem.201002111
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap / dichloromethane / 20 °C
2: 10% palladium on activated charcoal; hydrogen / 6 h
3: potassium carbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
With
dmap; 10% palladium on activated charcoal; hydrogen; potassium carbonate;
In
dichloromethane; acetonitrile;
DOI:10.1002/chem.201002111
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium tetrahydroborate / methanol / 4 h
2: dmap / dichloromethane / 20 °C
3: dmap / dichloromethane / Cooling with ice; Reflux
4: potassium carbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
With
dmap; sodium tetrahydroborate; potassium carbonate;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1002/chem.201002111
