2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-4-O-diphenylphosphono-6-O-(2,2,2-trichloroethoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-3-O-<(R)-3-(2,2,2-tr..)..>..>...

Base Information

• Chemical Name: 2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-4-O-diphenylphosphono-6-O-(2,2,2-trichloroethoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-3-O-<(R)-3-(2,2,2-tr..)..>..>...
• CAS No.: 118638-34-9
• Molecular Formula: C₁₀₃H₁₃₉Cl₉N₂O₂₈P₂
• Molecular Weight: 2234.26

Synonyms:

Chemical Property of 2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-4-O-diphenylphosphono-6-O-(2,2,2-trichloroethoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-3-O-<(R)-3-(2,2,2-tr..)..>..>...

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-4-O-diphenylphosphono-6-O-(2,2,2-trichloroethoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-3-O-<(R)-3-(2,2,2-tr..)..>..>...

There total 1 articles about 2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-4-O-diphenylphosphono-6-O-(2,2,2-trichloroethoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-3-O-<(R)-3-(2,2,2-tr..)..>..>... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-α-D-glucopyranoside (118638-75-8) + (R)-3-(2,2,2-Trichloro-ethoxycarbonyloxy)-tetradecanoic acid (2R,3R,4R,5S,6R)-2-bromo-5-(diphenoxy-phosphoryloxy)-3-(2,2,2-trichloro-ethoxycarbonylamino)-6-(2,2,2-trichloro-ethoxycarbonyloxymethyl)-tetrahydro-pyran-4-yl ester (137600-40-9) → 2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-4-O-diphenylphosphono-6-O-(2,2,2-trichloroethoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-3-O-<(R)-3-(2,2,2-tr..)..>..>... (118638-34-9)

Guidance literature:

With calcium sulfate; mercury(II) cyanide; In dichloromethane; for 18h; Yield given; Heating;

DOI:10.1248/cpb.39.1994

Reference yield:

Tetradecanoic acid benzotriazol-1-yl ester (125678-66-2) + 2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-4-O-diphenylphosphono-6-O-(2,2,2-trichloroethoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-3-O-<(R)-3-(2,2,2-tr..)..>..>... (118638-34-9) → 2-(diphenylphosphonooxy)ethyl 2-deoxy-6-O-(2-deoxy-4-O-diphenylphosphono-3-O-tetradecanoyl-2-tetradecanoylamino-β-D-glucopyranosyl)-3-O-tetradecanoyl-2-tetradecanoylamino-α-D-glucopyranoside (118638-37-2)

Guidance literature:

With 4-methyl-morpholine; acetic acid; zinc; Yield given. Multistep reaction; 1) r.t, 2 h, 2) THF, CH₂Cl₂, r.t., 13 h;

DOI:10.1248/cpb.39.1994

Reference yield:

(R)-3-Hydroxy-tetradecanoic acid benzotriazol-1-yl ester + 2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-4-O-diphenylphosphono-6-O-(2,2,2-trichloroethoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-3-O-<(R)-3-(2,2,2-tr..)..>..>... (118638-34-9) → 2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-4-O-diphenylphosphono-3-O-<(R)-3-hydroxytetradecanoyl>-2-<(R)-3-hydroxytetradecanoylamino>-β-D-glucopyranosyl>-α-D-glucopyra... (118638-35-0)

Guidance literature:

With 4-methyl-morpholine; acetic acid; zinc; Yield given. Multistep reaction; 1) r.t, 2 h, 2) THF, CH₂Cl₂, r.t.,13 h;

DOI:10.1248/cpb.39.1994

upstream raw materials:

2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-α-D-glucopyranoside

(R)-3-(2,2,2-Trichloro-ethoxycarbonyloxy)-tetradecanoic acid (2R,3R,4R,5S,6R)-2-bromo-5-(diphenoxy-phosphoryloxy)-3-(2,2,2-trichloro-ethoxycarbonylamino)-6-(2,2,2-trichloro-ethoxycarbonyloxymethyl)-tetrahydro-pyran-4-yl ester

Downstream raw materials:

2-(diphenylphosphonooxy)ethyl 2-deoxy-6-O-(2-deoxy-4-O-diphenylphosphono-3-O-tetradecanoyl-2-tetradecanoylamino-β-D-glucopyranosyl)-3-O-tetradecanoyl-2-tetradecanoylamino-α-D-glucopyranoside

2-(diphenylphosphonooxy)ethyl 3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-6-O-<2-deoxy-4-O-diphenylphosphono-3-O-<(R)-3-hydroxytetradecanoyl>-2-<(R)-3-hydroxytetradecanoylamino>-β-D-glucopyranosyl>-α-D-glucopyra...

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