Technology Process of C60H95N7O15
There total 17 articles about C60H95N7O15 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1021/ja109665t
- Guidance literature:
-
Multi-step reaction with 10 steps
1: methanol; N-ethyl-N,N-diisopropylamine / 20 °C / Inert atmosphere
2: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C
3: dicyclohexyl-carbodiimide / tetrahydrofuran / 3 h / 20 °C
4: sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / 20 °C
5: dicyclohexyl-carbodiimide / tetrahydrofuran / 3 h / 20 °C
6: sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / 20 °C
7: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 760.05 Torr
8: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 48 h / 20 °C
9: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
10: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C
With
methanol; palladium 10% on activated carbon; water; hydrogen; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ja109665t
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium periodate; ruthenium(III) chloride monohydrate / water; ethyl acetate; acetonitrile / 20 h / 20 °C
2: dicyclohexyl-carbodiimide / tetrahydrofuran / 48 h / 20 °C
3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C
With
sodium periodate; ruthenium(III) chloride monohydrate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; water; ethyl acetate; acetonitrile;
DOI:10.1021/ja109665t