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Technology Process of C16H18O2Si

C16H18O2Si

Base Information
  • Chemical Name:C16H18O2Si
  • CAS No.:1313753-62-6
  • Molecular Formula:C16H18O2Si
  • Molecular Weight:270.403
  • Hs Code.:
C<sub>16</sub>H<sub>18</sub>O<sub>2</sub>Si

Synonyms:

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Chemical Property of C16H18O2Si
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Technology Process of C16H18O2Si

There total 3 articles about C16H18O2Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

C<sub>18</sub>H<sub>22</sub>O<sub>2</sub>Si

C18H22O2Si

C<sub>16</sub>H<sub>18</sub>O<sub>2</sub>Si
1313753-62-6

C16H18O2Si

Guidance literature:
With gold(III) chloride; silver hexafluoro antimonate; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c1cc10920k

Reference yield:

C<sub>18</sub>H<sub>24</sub>O<sub>2</sub>Si

C18H24O2Si

C<sub>16</sub>H<sub>18</sub>O<sub>2</sub>Si
1313753-62-6

C16H18O2Si

Guidance literature:
Multi-step reaction with 2 steps
1: manganese(IV) oxide / dichloromethane; benzene / 18 h / 20 °C / Molecular sieve
2: gold(III) chloride; silver hexafluoro antimonate / dichloromethane / 12 h / 20 °C / Inert atmosphere
With manganese(IV) oxide; gold(III) chloride; silver hexafluoro antimonate; In dichloromethane; benzene; 2: Nazarov cyclization;
DOI:10.1039/c1cc10920k

Reference yield:

C<sub>14</sub>H<sub>16</sub>OSi
848220-57-5

C14H16OSi

C<sub>16</sub>H<sub>18</sub>O<sub>2</sub>Si
1313753-62-6

C16H18O2Si

Guidance literature:
Multi-step reaction with 3 steps
1.1: tert.-butyl lithium / tetrahydrofuran; hexane / -78 - 0 °C / Inert atmosphere
1.2: -78 °C / Inert atmosphere
2.1: manganese(IV) oxide / dichloromethane; benzene / 18 h / 20 °C / Molecular sieve
3.1: gold(III) chloride; silver hexafluoro antimonate / dichloromethane / 12 h / 20 °C / Inert atmosphere
With manganese(IV) oxide; gold(III) chloride; silver hexafluoro antimonate; tert.-butyl lithium; In tetrahydrofuran; hexane; dichloromethane; benzene; 3.1: Nazarov cyclization;
DOI:10.1039/c1cc10920k
upstream raw materials:

C14H16OSi

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