C₃₂H₄₄N₂O₂

Base Information

Chemical Name:C₃₂H₄₄N₂O₂
CAS No.:102393-27-1
Molecular Formula:C₃₂H₄₄N₂O₂
Molecular Weight:488.714
Hs Code.:

C<sub>32</sub>H<sub>44</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₄₄N₂O₂

Chemical Property:

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Technology Process of C₃₂H₄₄N₂O₂

There total 18 articles about C₃₂H₄₄N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3022-16-0
1,4-bis(chloromethyl)-2,3,5,6-tetramethylbenzene

: 102393-27-1
C₃₂H₄₄N₂O₂

Guidance literature:: Multi-step reaction with 16 steps

1: 1.) Na / 1.) ethanol; 2.) ethanol, reflux, 0.5 h

2: H₂O, KOH / Heating

3: 94.7 percent / quinoline / 0.33 h / Heating

4: 89.4 percent / cc. H₂SO₄ / toluene

5: 89.6 percent / B₂H₆ / tetrahydrofuran

6: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

7: 97 percent / ethanol / 4 h / Heating

8: 98 percent / H₂O, KOH / ethanol / Heating

9: SOCl₂ / Heating

10: SnCl₂ / CH₂Cl₂; nitromethane / Ambient temperature

11: B₂H₆ / tetrahydrofuran

12: PhCH₂ONa / Heating

13: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

14: dimethylformamide / Heating

15: POCl₃ / CH₂Cl₂

16: NaHCO₃ / H₂O / Heating

With quinoline; potassium hydroxide; thionyl chloride; sulfuric acid; water; hydrogen bromide; hydrogen; sodium; sodium hydrogencarbonate; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 102393-10-2
4-[4-(3-Chlorocarbonyl-propyl)-2,3,5,6-tetramethyl-phenyl]-butyryl chloride

: 102393-27-1
C₃₂H₄₄N₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1: SnCl₂ / CH₂Cl₂; nitromethane / Ambient temperature

2: B₂H₆ / tetrahydrofuran

3: PhCH₂ONa / Heating

4: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

5: dimethylformamide / Heating

6: POCl₃ / CH₂Cl₂

7: NaHCO₃ / H₂O / Heating

With hydrogen; sodium hydrogencarbonate; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 102393-13-5
C₃₆H₄₈N₂O₆

: 102393-27-1
C₃₂H₄₄N₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1: B₂H₆ / tetrahydrofuran

2: PhCH₂ONa / Heating

3: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

4: dimethylformamide / Heating

5: POCl₃ / CH₂Cl₂

6: NaHCO₃ / H₂O / Heating

With hydrogen; sodium hydrogencarbonate; triethylamine; sodium phenyl-methanolate; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;