Technology Process of C22H44N4O10
There total 6 articles about C22H44N4O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
20 % Pd(OH)2/C; hydrogen;
In
water; acetic acid;
DOI:10.1038/ja.2010.110
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium methylate / tetrahydrofuran; methanol
2: sodium hydroxide; trimethylphosphane / tetrahydrofuran
3: 20 % Pd(OH)2/C; hydrogen / water; acetic acid
With
20 % Pd(OH)2/C; hydrogen; sodium methylate; sodium hydroxide; trimethylphosphane;
In
tetrahydrofuran; methanol; water; acetic acid;
2: Staudinger reduction;
DOI:10.1038/ja.2010.110
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran
2: N-iodo-succinimide; trifluorormethanesulfonic acid / diethyl ether; dichloromethane
3: sodium methylate / tetrahydrofuran; methanol
4: sodium hydroxide; trimethylphosphane / tetrahydrofuran
5: 20 % Pd(OH)2/C; hydrogen / water; acetic acid
With
N-iodo-succinimide; trifluorormethanesulfonic acid; 20 % Pd(OH)2/C; hydrogen; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydroxide; trimethylphosphane;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetic acid;
4: Staudinger reduction;
DOI:10.1038/ja.2010.110
