Technology Process of 5,15-bis(2,3,5,6-tetrafluorophenyl)-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II)
There total 5 articles about 5,15-bis(2,3,5,6-tetrafluorophenyl)-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
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1350823-58-3
5,15-bis(2,3,5,6-tetrafluorophenyl)-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II)
- Guidance literature:
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Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / 1 h / 0 °C / Inert atmosphere
2.1: methanol / 6 h / -25 - 20 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: zinc(II) acetate dihydrate / methanol; chloroform / 0.33 h / Reflux
With
zinc(II) acetate dihydrate; trifluoroacetic acid;
In
methanol; chloroform;
DOI:10.1039/c1dt10880h
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1350823-58-3
5,15-bis(2,3,5,6-tetrafluorophenyl)-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II)
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methanol / 6 h / -25 - 20 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: zinc(II) acetate dihydrate / methanol; chloroform / 0.33 h / Reflux
With
zinc(II) acetate dihydrate;
In
methanol; chloroform;
DOI:10.1039/c1dt10880h
-
-
1350823-58-3
5,15-bis(2,3,5,6-tetrafluorophenyl)-2,8,12,18-tetra(n-hexyl)-3,7,13,17-tetramethylporphyrin zinc(II)
- Guidance literature:
-
With
zinc(II) acetate dihydrate;
In
methanol; chloroform;
for 0.333333h;
Reflux;
DOI:10.1039/c1dt10880h
