Benzenemethanol, alpha-[[2-(acetyloxy)-2-phenylethoxy]methyl]-

Base Information

Chemical Name:Benzenemethanol, alpha-[[2-(acetyloxy)-2-phenylethoxy]methyl]-
CAS No.:83072-51-9
Molecular Formula:C₁₈H₂₀O₄
Molecular Weight:300.354
Hs Code.:
DSSTox Substance ID:DTXSID001192620

Synonyms:DTXSID001192620;Benzenemethanol, alpha-[[2-(acetyloxy)-2-phenylethoxy]methyl]-;83072-51-9

Suppliers and Price of Benzenemethanol, alpha-[[2-(acetyloxy)-2-phenylethoxy]methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenemethanol, alpha-[[2-(acetyloxy)-2-phenylethoxy]methyl]-

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:300.13615911
Heavy Atom Count:22
Complexity:319

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)OC(COCC(C1=CC=CC=C1)O)C2=CC=CC=C2

Technology Process of Benzenemethanol, alpha-[[2-(acetyloxy)-2-phenylethoxy]methyl]-

There total 3 articles about Benzenemethanol, alpha-[[2-(acetyloxy)-2-phenylethoxy]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 108-24-7
acetic anhydride

: 83072-49-5
2,2'-Oxybis(1-phenylethanol)

: 83072-51-9
2-(2-Hydroxy-2-phenylethoxy)-1-phenylethylacetat

Guidance literature:: In benzene; for 5h; Heating;
DOI:10.1002/ardp.19823150806

Reference yield:

: 33868-49-4
acetonyl phenacyl ether

: 83072-51-9
2-(2-Hydroxy-2-phenylethoxy)-1-phenylethylacetat

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol / 0.25 h

2: 93 percent / benzene / 5 h / Heating

With hydrogen; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1002/ardp.19823150806

Reference yield:

: 3282-32-4
2-diazo-acetophenone

: 83072-51-9
2-(2-Hydroxy-2-phenylethoxy)-1-phenylethylacetat

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) BF₃-etherat, 2.) 4-toluenesulfonic acid / 1.) benzene, 15 deg C, 2.) dioxane, reflux, 6 h

2: H₂ / Pd/C / ethanol / 0.25 h

3: 93 percent / benzene / 5 h / Heating

With boron trifluoride diethyl etherate; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1002/ardp.19823150806