(3S,4S)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(3-hydroxypropyl)pyrrolidin-2-one

Base Information

Chemical Name:(3S,4S)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(3-hydroxypropyl)pyrrolidin-2-one
CAS No.:1365541-69-0
Molecular Formula:C₃₅H₅₅NO₄Si₂
Molecular Weight:609.997
Hs Code.:

(3S,4S)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(3-hydroxypropyl)pyrrolidin-2-one

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Chemical Property of (3S,4S)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(3-hydroxypropyl)pyrrolidin-2-one

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Technology Process of (3S,4S)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(3-hydroxypropyl)pyrrolidin-2-one

There total 9 articles about (3S,4S)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(3-hydroxypropyl)pyrrolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₃H₆₈BNO₃Si₂

: 1365541-69-0
(3S,4S)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(3-hydroxypropyl)pyrrolidin-2-one

Guidance literature:: With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; ethanol; water; at 20 ℃; for 2h;
DOI:10.1021/jm201620t

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 1365541-69-0
(3S,4S)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(3-hydroxypropyl)pyrrolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 - 25 °C

2: tetrahydrofuran / 6 h / 20 - 80 °C

3: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; ethanol; water / 2 h / 20 °C

With dihydrogen peroxide; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm201620t

Reference yield:

: C₁₄H₁₄O₃

: 1365541-69-0
(3S,4S)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(3-hydroxypropyl)pyrrolidin-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: methanol; sodium tetrahydroborate / tetrahydrofuran / 2 h / 20 °C

2: 1-butyl-3-methylimidazolium Tetrafluoroborate / 0.58 h / 180 °C / Microwave irradiation

3: triethylamine / dichloromethane / 0 - 25 °C

4: tetrahydrofuran / 6 h / 20 - 80 °C

5: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; ethanol; water / 2 h / 20 °C

With methanol; sodium tetrahydroborate; dihydrogen peroxide; triethylamine; 1-butyl-3-methylimidazolium Tetrafluoroborate; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm201620t