Technology Process of (Z)-1-allyloxy-3-(prop-1-en-1-yl)benzene
There total 6 articles about (Z)-1-allyloxy-3-(prop-1-en-1-yl)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
ethyltriphenylphosphonium bromide;
With
potassium tert-butylate;
In
tetrahydrofuran;
at 20 ℃;
for 3h;
Inert atmosphere;
3-allyloxy-benzaldehyde;
In
tetrahydrofuran;
at -78 - 20 ℃;
for 15h;
optical yield given as %de;
Inert atmosphere;
DOI:10.1039/c2cc17572j
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: oxygen / dimethyl sulfoxide / 24 h / 20 °C / 1500.15 Torr / pH 6 / aq. buffer; Enzymatic reaction
2.1: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
2.2: 15 h / -78 - 20 °C / Inert atmosphere
With
potassium tert-butylate; oxygen;
In
tetrahydrofuran; dimethyl sulfoxide;
2.2: Wittig reaction;
DOI:10.1039/c2cc17572j
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: oxygen / dimethyl sulfoxide / 24 h / 20 °C / 1500.15 Torr / pH 6 / aq. buffer; Enzymatic reaction
2.1: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
2.2: 15 h / -78 - 20 °C / Inert atmosphere
With
potassium tert-butylate; oxygen;
In
tetrahydrofuran; dimethyl sulfoxide;
2.2: Wittig reaction;
DOI:10.1039/c2cc17572j
