6-(4-methylphenyl)-5H-dibenzo<1,3>diazepine

Base Information

Chemical Name:6-(4-methylphenyl)-5H-dibenzo<1,3>diazepine
CAS No.:4509-47-1
Molecular Formula:C₂₀H₁₆N₂
Molecular Weight:284.36
Hs Code.:

6-(4-methylphenyl)-5H-dibenzo<d,f><1,3>diazepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(4-methylphenyl)-5H-dibenzo<1,3>diazepine

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Technology Process of 6-(4-methylphenyl)-5H-dibenzo<1,3>diazepine

There total 3 articles about 6-(4-methylphenyl)-5H-dibenzo<1,3>diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1454-80-4
1,1'-biphenyl-2,2'-diamine

: 4-Methyl-thiobenzimidic acid methyl ester; hydriodide

: 4509-47-1
6-(4-methylphenyl)-5H-dibenzo<1,3>diazepine

Guidance literature:: In ethanol; for 3h; Heating;
DOI:10.1080/00397919708004101

Reference yield:

: 2362-62-1
4-methylthiobenzamide

: 4509-47-1
6-(4-methylphenyl)-5H-dibenzo<1,3>diazepine

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 2 h / 60 °C

2: 81 percent / ethanol / 3 h / Heating

In ethanol; acetone;
DOI:10.1080/00397919708004101

Reference yield:

: 4509-47-1
6-(4-methylphenyl)-5H-dibenzo<1,3>diazepine

Guidance literature:: <4-Methyl-phenyl>-formimidsaeure-aethylester-Hydrochlorid, 1) 2.2'-Diamino-biphenyl, 65grad, 15 Min. -> 20grad, 12-16 h, 2) aq. NaOH, Diaethylaether; Ausb. 17,5percent;

upstream raw materials:

1,1'-biphenyl-2,2'-diamine

4-methylthiobenzamide

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