2'-phenyl-spiro

Base Information

• Chemical Name: 2'-phenyl-spiro
• CAS No.: 19576-01-3
• Molecular Formula: C₂₂H₁₆O
• Molecular Weight: 296.368

Synonyms:

Chemical Property of 2'-phenyl-spiro

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2'-phenyl-spiro

There total 2 articles about 2'-phenyl-spiro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + carbene anthronylidene (19584-41-9) → 2'-phenyl-spiro (19576-01-3)

Guidance literature:

In benzene; Rate constant;

DOI:10.1021/jo00252a023

Reference yield:

→ 2'-phenyl-spiro (19576-01-3)

Guidance literature:

10-Diazoanthron, Styrol;

Reference yield: 71.0%

2'-phenyl-spiro (19576-01-3) + acetic anhydride (108-24-7) → 10-acetoxy-9-styrylanthracene (76664-86-3)

Guidance literature:

With sulfuric acid; at 95 ℃; for 2h;

upstream raw materials:

styrene

carbene anthronylidene

Downstream raw materials:

10-acetoxy-9-styrylanthracene

10-acetoxy-9-(2-acetoxy-2-phenylethyl)anthracene

Acetic acid 10-(2-methoxy-2-phenyl-ethyl)-anthracen-9-yl ester

10-methylene-9,10-dihydroanthryl-9-spirophenylcyclopropane

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