1-<2-(3-benzyloxy-4-methoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

Base Information

Chemical Name:1-<2-(3-benzyloxy-4-methoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone
CAS No.:115262-46-9
Molecular Formula:C₂₃H₂₉NO₄
Molecular Weight:383.488
Hs Code.:

Synonyms:

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Chemical Property of 1-<2-(3-benzyloxy-4-methoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

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Technology Process of 1-<2-(3-benzyloxy-4-methoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

There total 1 articles about 1-<2-(3-benzyloxy-4-methoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 115262-45-8,115262-74-3
1-(3-benzyloxy-4-methoxyphenyl)-2-<3-(1,1-ethylenedioxyethyl)piperidino>ethanol

: 115262-46-9,115262-75-4
1-<2-(3-benzyloxy-4-methoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

Guidance literature:: With hydrogenchloride; at 40 ℃; for 2.5h;

Reference yield: 76.0%

: 115262-46-9,115262-75-4
1-<2-(3-benzyloxy-4-methoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

: 115262-47-0
1-<2-(3-benzyloxy-4-methoxyphenyl)-2-hydroxyethyl>-1,2,3,4-tetrahydro-5-pyridyl methyl ketone

: 115262-48-1,115262-76-5
5-acetyl-1-<2-(3-benzyloxy-4-methoxyphenyl)-2-hydroxyethyl>-piperidone

Guidance literature:: With Hg(OAc)2*EDTA; In acetic acid; for 1.5h; Heating;

Reference yield:

: 115262-46-9,115262-75-4
1-<2-(3-benzyloxy-4-methoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

: 115262-49-2
5-acetyl-1-(3-hydroxy-4-methoxyphenethyl)-2-piperidone

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / Hg(OAc)2-EDTA / aq. acetic acid / 1.5 h / Heating

2: 71 percent / H₂ / Pd-C (10percent) / ethanol; aq. HClO₄ / 42 h / 35 °C / 2280 - 2850 Torr

With Hg(OAc)2*EDTA; hydrogen; palladium on activated charcoal; In perchloric acid; ethanol; acetic acid;