C₂₀H₂₂O₃

Base Information

Chemical Name:C₂₀H₂₂O₃
CAS No.:1579954-67-8
Molecular Formula:C₂₀H₂₂O₃
Molecular Weight:310.393
Hs Code.:

C<sub>20</sub>H<sub>22</sub>O<sub>3</sub>

Synonyms:

Suppliers and Price of C₂₀H₂₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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Technology Process of C₂₀H₂₂O₃

There total 15 articles about C₂₀H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1579954-62-3
(3R,E)-3-(Benzyloxy)-6-(tetrahydropyran-2-yloxy)-hex-4-enal

: 100-51-6,185532-71-2
benzyl alcohol

: 1579954-66-7
C₂₀H₂₂O₃

: 1579954-67-8
C₂₀H₂₂O₃

: 1579954-68-9
C₂₀H₂₂O₃

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); In tetrahydrofuran; at 20 ℃; for 1.5h; Overall yield = 47 %; Overall yield = 144 mg; Inert atmosphere;
DOI:10.3987/COM-13-12896

Reference yield:

: 1579954-58-7
(3R,Z)-3-(benzyloxy)-6-(tetrahydropyran-2-yloxy)-hex-4-enal

: 100-51-6,185532-71-2
benzyl alcohol

: 1579954-66-7
C₂₀H₂₂O₃

: 1579954-67-8
C₂₀H₂₂O₃

: 1579954-68-9
C₂₀H₂₂O₃

: C₂₀H₂₂O₃

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); In tetrahydrofuran; at 20 ℃; for 1.5h; Overall yield = 42 %; Inert atmosphere;
DOI:10.3987/COM-13-12896

Reference yield:

: 1579954-54-3
(R)-6-(tert-butyldimethylsilyloxy)-1-(tetrahydropyran-2-yloxy)-hex-2-yn-4-ol

: 1579954-66-7
C₂₀H₂₂O₃

: 1579954-67-8
C₂₀H₂₂O₃

: C₂₀H₂₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen / methanol / 19 h / 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C

2.2: 5 h / Reflux

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere

4.1: 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

4.2: 0.25 h / 20 °C / Molecular sieve; Inert atmosphere

5.1: dichloro bis(acetonitrile) palladium(II) / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

With dichloro bis(acetonitrile) palladium(II); tetrabutyl ammonium fluoride; hydrogen; sodium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; dichloromethane; mineral oil;
DOI:10.3987/COM-13-12896