3-[(cyclopentylsulfanyl)methyl]-4-methoxy-N-phenylbenzenecarboximidamide

Base Information

Chemical Name:3-[(cyclopentylsulfanyl)methyl]-4-methoxy-N-phenylbenzenecarboximidamide
CAS No.:1569736-45-3
Molecular Formula:C₂₀H₂₄N₂OS
Molecular Weight:340.489
Hs Code.:

Synonyms:

Suppliers and Price of 3-[(cyclopentylsulfanyl)methyl]-4-methoxy-N-phenylbenzenecarboximidamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-[(cyclopentylsulfanyl)methyl]-4-methoxy-N-phenylbenzenecarboximidamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-[(cyclopentylsulfanyl)methyl]-4-methoxy-N-phenylbenzenecarboximidamide

There total 4 articles about 3-[(cyclopentylsulfanyl)methyl]-4-methoxy-N-phenylbenzenecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1509142-60-2
3-[(cyclopentylsulfanyl)methyl]-4-methoxybenzonitrile

: 62-53-3
aniline

: 1569736-45-3
3-[(cyclopentylsulfanyl)methyl]-4-methoxy-N-phenylbenzenecarboximidamide

Guidance literature:: aniline; With trimethylaluminum; In toluene; at 20 ℃; for 0.333333h; Inert atmosphere; Cooling with ice;

3-[(cyclopentylsulfanyl)methyl]-4-methoxybenzonitrile; In toluene; at 95 ℃; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ml400519h

Reference yield:

: 1569736-41-9
(5-chloro-2-methoxybenzyl)(cyclopentyl)sulfane

: 1569736-45-3
3-[(cyclopentylsulfanyl)methyl]-4-methoxy-N-phenylbenzenecarboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl acetamide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; XPhos; zinc / 2 h / 150 °C / Inert atmosphere; Microwave irradiation

2.1: trimethylaluminum / toluene / 0.33 h / 20 °C / Inert atmosphere; Cooling with ice

2.2: 95 °C / Inert atmosphere; Microwave irradiation

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; N,N-dimethyl acetamide; trimethylaluminum; zinc; XPhos; In toluene;
DOI:10.1021/ml400519h

Reference yield:

: 1679-07-8
cyclopentylthiol

: 1569736-45-3
3-[(cyclopentylsulfanyl)methyl]-4-methoxy-N-phenylbenzenecarboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C / Inert atmosphere

2.1: N,N-dimethyl acetamide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; XPhos; zinc / 2 h / 150 °C / Inert atmosphere; Microwave irradiation

3.1: trimethylaluminum / toluene / 0.33 h / 20 °C / Inert atmosphere; Cooling with ice

3.2: 95 °C / Inert atmosphere; Microwave irradiation

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; N,N-dimethyl acetamide; trimethylaluminum; potassium carbonate; zinc; XPhos; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/ml400519h