Technology Process of C23H30N4O5S
There total 9 articles about C23H30N4O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ozone;
In
methanol; water; acetone;
at 20 ℃;
for 1h;
DOI:10.1021/jm301404a
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride; tin(ll) chloride / ethanol / 1 h / 20 - 80 °C
2.1: sodium cyanoborohydride; acetic acid / methanol / 19 h / -15 - 20 °C
3.1: trifluoroacetic acid / dichloromethane; methanol / 22 h / 20 °C
4.1: sodium hydride / tetrahydrofuran / 0.5 h / Reflux
4.2: 1.5 h / 20 °C / Reflux
5.1: ozone / methanol; water; acetone / 1 h / 20 °C
With
hydrogenchloride; sodium hydride; sodium cyanoborohydride; ozone; acetic acid; trifluoroacetic acid; tin(ll) chloride;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetone;
DOI:10.1021/jm301404a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium cyanoborohydride; acetic acid / methanol / 19 h / -15 - 20 °C
2.1: trifluoroacetic acid / dichloromethane; methanol / 22 h / 20 °C
3.1: sodium hydride / tetrahydrofuran / 0.5 h / Reflux
3.2: 1.5 h / 20 °C / Reflux
4.1: ozone / methanol; water; acetone / 1 h / 20 °C
With
sodium hydride; sodium cyanoborohydride; ozone; acetic acid; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1021/jm301404a
